[1-(4-benzyloxycarbonylamino-benzyl)-3,5-dimethyl-1H-pyrazol-4-yl]-acetic acid

Base Information

Chemical Name:[1-(4-benzyloxycarbonylamino-benzyl)-3,5-dimethyl-1H-pyrazol-4-yl]-acetic acid
CAS No.:1322082-81-4
Molecular Formula:C₂₂H₂₃N₃O₄
Molecular Weight:393.442
Hs Code.:

Synonyms:[1-(4-benzyloxycarbonylamino-benzyl)-3,5-dimethyl-1H-pyrazol-4-yl]-acetic acid

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Chemical Property of [1-(4-benzyloxycarbonylamino-benzyl)-3,5-dimethyl-1H-pyrazol-4-yl]-acetic acid

Chemical Property:

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Technology Process of [1-(4-benzyloxycarbonylamino-benzyl)-3,5-dimethyl-1H-pyrazol-4-yl]-acetic acid

There total 7 articles about [1-(4-benzyloxycarbonylamino-benzyl)-3,5-dimethyl-1H-pyrazol-4-yl]-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₂₅N₃O₄

: 1322082-81-4
[1-(4-benzyloxycarbonylamino-benzyl)-3,5-dimethyl-1H-pyrazol-4-yl]-acetic acid

Guidance literature:: C₂₃H₂₅N₃O₄; With water; sodium hydroxide; In methanol;

With hydrogenchloride; In methanol; water;

Reference yield:

: 32701-82-9
(1-benzyl-3,5-dimethyl-1H-pyrazol-4-yl)acetic acid

: 1322082-81-4
[1-(4-benzyloxycarbonylamino-benzyl)-3,5-dimethyl-1H-pyrazol-4-yl]-acetic acid

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogenchloride / 18 h / 20 °C

2: nitric acid / sulfuric acid / 0.33 h / -7 - 20 °C

3: hydrogen / palladium 10% on activated carbon / methanol

4: N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 20 °C

5: sodium hydroxide; water / methanol

With water; hydrogen; nitric acid; N-ethyl-N,N-diisopropylamine; sodium hydroxide; hydrogenchloride; sulfuric acid; palladium 10% on activated carbon; In methanol; dichloromethane;

Reference yield:

: 1283378-96-0
(1-benzyl-3,5-dimethyl-1H-pyrazol-4-yl)-acetic acid methyl ester

: 1322082-81-4
[1-(4-benzyloxycarbonylamino-benzyl)-3,5-dimethyl-1H-pyrazol-4-yl]-acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1: nitric acid / sulfuric acid / 0.33 h / -7 - 20 °C

2: hydrogen / palladium 10% on activated carbon / methanol

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 20 °C

4: sodium hydroxide; water / methanol

With water; hydrogen; nitric acid; N-ethyl-N,N-diisopropylamine; sodium hydroxide; sulfuric acid; palladium 10% on activated carbon; In methanol; dichloromethane;