rac-bernumicine

Base Information

Chemical Name:rac-bernumicine
CAS No.:350586-87-7
Molecular Formula:C₂₀H₂₅NO₄
Molecular Weight:343.423
Hs Code.:

Synonyms:rac-bernumicine

Suppliers and Price of rac-bernumicine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of rac-bernumicine

Chemical Property:

Purity/Quality:

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Technology Process of rac-bernumicine

There total 6 articles about rac-bernumicine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 93-03-8
(3,4-dimethoxyphenyl)methanol

: 89-31-6,20405-58-7,76419-97-1,101467-40-7
rac-salsoline

: 350586-87-7
rac-bernumicine

Guidance literature:: (3,4-dimethoxyphenyl)methanol; With n-butyllithium; In tetrahydrofuran; hexane; at 20 ℃; for 0.0833333h;

With p-toluenesulfonyl chloride; In tetrahydrofuran; hexane; at 20 ℃; for 0.25h;

rac-salsoline; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; hexane; dichloromethane; at 20 ℃; for 360h;

Reference yield:

: 2426-87-1
3-methoxy-4-(phenylmethoxy)benzaldehyde

: 350586-87-7
rac-bernumicine

Guidance literature:: Multi-step reaction with 6 steps

1.1: 100 percent / NH₄OAc / Heating

2.1: 78 percent / LiAlH₄ / tetrahydrofuran / 0.5 h / Heating

3.1: 6.96 g / aq. K₂CO₃ / 1.5 h / 20 °C

4.1: 100 percent / p-toluenesulfonic acid / CH₂Cl₂ / Heating

5.1: 100 percent / H₂; HCO₂H / 10 percent Pd/C / methanol / 30 h / 20 °C / 760 Torr

6.1: n-BuLi / tetrahydrofuran; hexane / 0.08 h / 20 °C

6.2: p-toluenesulfonyl chloride / tetrahydrofuran; hexane / 0.25 h / 20 °C

6.3: 76 percent / diisopropylethylamine / tetrahydrofuran; hexane; CH₂Cl₂ / 360 h / 20 °C

With lithium aluminium tetrahydride; n-butyllithium; formic acid; ammonium acetate; hydrogen; potassium carbonate; toluene-4-sulfonic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; hexane; dichloromethane;

Reference yield:

: 63909-29-5,55507-05-6
3-benzyloxy-4-methoxy-β-nitrostyrene

: 350586-87-7
rac-bernumicine

Guidance literature:: Multi-step reaction with 5 steps

1.1: 78 percent / LiAlH₄ / tetrahydrofuran / 0.5 h / Heating

2.1: 6.96 g / aq. K₂CO₃ / 1.5 h / 20 °C

3.1: 100 percent / p-toluenesulfonic acid / CH₂Cl₂ / Heating

4.1: 100 percent / H₂; HCO₂H / 10 percent Pd/C / methanol / 30 h / 20 °C / 760 Torr

5.1: n-BuLi / tetrahydrofuran; hexane / 0.08 h / 20 °C

5.2: p-toluenesulfonyl chloride / tetrahydrofuran; hexane / 0.25 h / 20 °C

5.3: 76 percent / diisopropylethylamine / tetrahydrofuran; hexane; CH₂Cl₂ / 360 h / 20 °C

With lithium aluminium tetrahydride; n-butyllithium; formic acid; hydrogen; potassium carbonate; toluene-4-sulfonic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; hexane; dichloromethane;