4-Amino-N-(4-benzyl-morpholin-2-ylmethyl)-5-chloro-2-[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propoxy]-benzamide

Base Information

• Chemical Name: 4-Amino-N-(4-benzyl-morpholin-2-ylmethyl)-5-chloro-2-[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propoxy]-benzamide
• CAS No.: 144256-62-2
• Molecular Formula: C₃₀H₃₁ClN₄O₅
• Molecular Weight: 563.053

Synonyms:4-Amino-N-(4-benzyl-morpholin-2-ylmethyl)-5-chloro-2-[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propoxy]-benzamide

Chemical Property of 4-Amino-N-(4-benzyl-morpholin-2-ylmethyl)-5-chloro-2-[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propoxy]-benzamide

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Technology Process of 4-Amino-N-(4-benzyl-morpholin-2-ylmethyl)-5-chloro-2-[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propoxy]-benzamide

There total 1 articles about 4-Amino-N-(4-benzyl-morpholin-2-ylmethyl)-5-chloro-2-[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propoxy]-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

4-amino-N-<(4-benzyl-2-morpholinyl)methyl>-5-chloro-2-hydroxybenzamide (112885-63-9) → 4-Amino-N-(4-benzyl-morpholin-2-ylmethyl)-5-chloro-2-[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propoxy]-benzamide (144256-62-2)

Guidance literature:

With sodium hydroxide; tetrabutylammomium bromide; In dichloromethane; for 15h; Ambient temperature;

DOI:10.1248/cpb.40.1470

Reference yield: 97.0%

4-Amino-N-(4-benzyl-morpholin-2-ylmethyl)-5-chloro-2-[3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propoxy]-benzamide (144256-62-2) → 4-amino-2-(3-aminopropoxy)-N-<(4-benzyl-2-morpholinyl)methyl>-5-chlorobenzamide (112885-89-9)

Guidance literature:

With hydrazine hydrate; In ethanol; for 2h; Heating;

DOI:10.1248/cpb.40.1470

upstream raw materials:

4-amino-N-<(4-benzyl-2-morpholinyl)methyl>-5-chloro-2-hydroxybenzamide

Downstream raw materials:

4-amino-2-(3-aminopropoxy)-N-<(4-benzyl-2-morpholinyl)methyl>-5-chlorobenzamide

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