1,6-Anhydro-2-azido-3-O-benzyl-4-O--2-desoxy-β-D-glucopyranose

Base Information

Chemical Name:1,6-Anhydro-2-azido-3-O-benzyl-4-O--2-desoxy-β-D-glucopyranose
CAS No.:97783-75-0
Molecular Formula:C₂₆H₂₈N₆O₉
Molecular Weight:568.543
Hs Code.:

1,6-Anhydro-2-azido-3-O-benzyl-4-O-<benzyl-(2-azido-2-desoxy-β-D-mannopyranosyl)uronat>-2-desoxy-β-D-glucopyranose

Synonyms:1,6-Anhydro-2-azido-3-O-benzyl-4-O--2-desoxy-β-D-glucopyranose

Suppliers and Price of 1,6-Anhydro-2-azido-3-O-benzyl-4-O--2-desoxy-β-D-glucopyranose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,6-Anhydro-2-azido-3-O-benzyl-4-O--2-desoxy-β-D-glucopyranose

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,6-Anhydro-2-azido-3-O-benzyl-4-O--2-desoxy-β-D-glucopyranose

There total 6 articles about 1,6-Anhydro-2-azido-3-O-benzyl-4-O--2-desoxy-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 908094-04-2
phenyldiazomethane

: 95451-86-8
1,6-anhydro-2-azido-4-O-<(2-azido-2-deoxy-β-D-mannopyranosyl)uronic acid>-3-O-benzyl-2-deoxy-β-D-glucopyranose

: 97783-75-0
1,6-Anhydro-2-azido-3-O-benzyl-4-O--2-desoxy-β-D-glucopyranose

Guidance literature:: In methanol; diethyl ether; Ambient temperature;
DOI:10.1016/0008-6215(86)80006-4

Reference yield:

: 55682-57-0
1,6-anhydro-2-azido-3-O-benzyl-2-deoxy-β-D-glucopyranose

: 97783-75-0
1,6-Anhydro-2-azido-3-O-benzyl-4-O--2-desoxy-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) silver silicate, molecular sieves 4 Angstroem / 1.) toluol, 3 h, r.t., 2.) toluol

2: 97 percent / 0.1 M NaOMe / methanol / 8 h / Ambient temperature

3: 82 percent / O₂ / Pt (Adam's-katalysator) / H₂O; propan-1-ol / 6 h / 80 °C / NaHCO₃, pH 7.5

4: 62 percent / diethyl ether; methanol / Ambient temperature

With silver silicate; 4 A molecular sieve; oxygen; sodium methylate; platinum(IV) oxide; In methanol; propan-1-ol; diethyl ether; water;
DOI:10.1016/0008-6215(86)80006-4

Reference yield:

: 95451-93-7
3,4,6-Tri-O-acetyl-2-azido-2-deoxy-α-D-mannopyranosyl bromide

: 97783-75-0
1,6-Anhydro-2-azido-3-O-benzyl-4-O--2-desoxy-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) silver silicate, molecular sieves 4 Angstroem / 1.) toluol, 3 h, r.t., 2.) toluol

2: 97 percent / 0.1 M NaOMe / methanol / 8 h / Ambient temperature

3: 82 percent / O₂ / Pt (Adam's-katalysator) / H₂O; propan-1-ol / 6 h / 80 °C / NaHCO₃, pH 7.5

4: 62 percent / diethyl ether; methanol / Ambient temperature

With silver silicate; 4 A molecular sieve; oxygen; sodium methylate; platinum(IV) oxide; In methanol; propan-1-ol; diethyl ether; water;
DOI:10.1016/0008-6215(86)80006-4