benzyl (R)-4-((S)-2-((R)-2-(((2S,3R,4R,5S,6R)-3-acetamido-2-(benzyloxy)-5-hydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-4-yl)oxy)propanamido)propanamido)-5-amino-5-oxopentanoate

Base Information

• Chemical Name: benzyl (R)-4-((S)-2-((R)-2-(((2S,3R,4R,5S,6R)-3-acetamido-2-(benzyloxy)-5-hydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-4-yl)oxy)propanamido)propanamido)-5-amino-5-oxopentanoate
• CAS No.: 62928-83-0
• Molecular Formula: C₃₃H₄₄N₄O₁₁
• Molecular Weight: 672.733

Synonyms:benzyl (R)-4-((S)-2-((R)-2-(((2S,3R,4R,5S,6R)-3-acetamido-2-(benzyloxy)-5-hydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-4-yl)oxy)propanamido)propanamido)-5-amino-5-oxopentanoate

Chemical Property of benzyl (R)-4-((S)-2-((R)-2-(((2S,3R,4R,5S,6R)-3-acetamido-2-(benzyloxy)-5-hydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-4-yl)oxy)propanamido)propanamido)-5-amino-5-oxopentanoate

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of benzyl (R)-4-((S)-2-((R)-2-(((2S,3R,4R,5S,6R)-3-acetamido-2-(benzyloxy)-5-hydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-4-yl)oxy)propanamido)propanamido)-5-amino-5-oxopentanoate

There total 25 articles about benzyl (R)-4-((S)-2-((R)-2-(((2S,3R,4R,5S,6R)-3-acetamido-2-(benzyloxy)-5-hydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-4-yl)oxy)propanamido)propanamido)-5-amino-5-oxopentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

N-acetyl-1-O-benzyl-4,6-O-benzylidene-α-muramyl-α-aminoisobutyryl-D-isoglutamine benzyl ester (71811-18-2) → benzyl 2-acetamido-2-deoxy-3-O-(D-2-propanoyl-L-alanyl-D-isoglutamine benzyl ester)-α-D-glucopyranoside (57816-11-2,62928-83-0,75283-21-5,76498-06-1,76498-09-4)

Guidance literature:

With acetic acid; for 0.5h; Heating;

DOI:10.1248/cpb.29.2215

Reference yield: 73.0%

benzyl (R)-4-((S)-2-((R)-2-(((4aR,6S,7R,8R,8aS)-7-acetamido-6-(benzyloxy)-2,2-dimethylhexahydropyrano[3,2-d][1,3]dioxin-8-yl)oxy)propanamido)propanamido)-5-amino-5-oxopentanoate (69323-69-9,75263-32-0,75283-18-0,77843-23-3,128779-65-7) → benzyl (R)-4-((S)-2-((R)-2-(((2S,3R,4R,5S,6R)-3-acetamido-2-(benzyloxy)-5-hydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-4-yl)oxy)propanamido)propanamido)-5-amino-5-oxopentanoate (62928-83-0)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere;

DOI:10.1021/acs.jmedchem.6b00681

Reference yield: 60.0%

benzyl N2-(N-acetyl-1-O-benzyl-4,6-O-benzylidene-α-D-muramoyl)-L-alanyl-D-isoglutaminate (59573-84-1) → benzyl (R)-4-((S)-2-((R)-2-(((2S,3R,4R,5S,6R)-3-acetamido-2-(benzyloxy)-5-hydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-4-yl)oxy)propanamido)propanamido)-5-amino-5-oxopentanoate (62928-83-0)

Guidance literature:

With acetic acid; In water; for 0.5h; Heating;

DOI:10.1002/hlca.19930760819

upstream raw materials:

N-<2-O-(benzyl 2-acetamido-2,3-dideoxy-4,6-O-isopropylidene-β-D-glucopyranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamine benzyl ester

benzyl 2-acetamido-3-O-(D-1-carboxyethyl)-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

N-acetyl-1-O-benzyl-4,6-O-benzylidene-α-muramyl-α-aminoisobutyryl-D-isoglutamine benzyl ester

benzyl N²-(N-acetyl-1-O-benzyl-4,6-O-benzylidene-α-D-muramoyl)-L-alanyl-D-isoglutaminate

Downstream raw materials:

N-<2-O-(benzyl 2-acetamido-6-O-< 5-(tert-butoxycarbonylamino)pentanoyl>-2,3-dideoxy-β-D-glucopyranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamine benzyl ester

N-<2-O-(benzyl 2-acetamido-6-O-< 8-(tert-butoxycarbonylamino)octanoyl>-2,3-dideoxy-β-D-glucopyranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamine benzyl ester

(R)-4-[(S)-2-((S)-2-{(2R,3R,4R,5S,6R)-3-Acetylamino-2-benzyloxy-6-[3-(6-chloro-2-methoxy-acridin-9-ylamino)-propionyloxymethyl]-5-hydroxy-tetrahydro-pyran-4-yloxy}-propionylamino)-propionylamino]-4-carbamoyl-butyric acid benzyl ester

(R)-4-[(S)-2-((S)-2-{(2R,3R,4R,5S,6R)-3-Acetylamino-6-[3-(acridin-9-ylamino)-propionyloxymethyl]-2-benzyloxy-5-hydroxy-tetrahydro-pyran-4-yloxy}-propionylamino)-propionylamino]-4-carbamoyl-butyric acid benzyl ester

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