C₃₅H₃₆N₆O₉

Base Information

Chemical Name:C₃₅H₃₆N₆O₉
CAS No.:476667-26-2
Molecular Formula:C₃₅H₃₆N₆O₉
Molecular Weight:684.706
Hs Code.:

C<sub>35</sub>H<sub>36</sub>N<sub>6</sub>O<sub>9</sub>

Synonyms:C₃₅H₃₆N₆O₉

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Chemical Property of C₃₅H₃₆N₆O₉

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Technology Process of C₃₅H₃₆N₆O₉

There total 8 articles about C₃₅H₃₆N₆O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 476667-20-6
C₁₉H₂₁N₃O₅

: 476667-24-0
(8-hydroxy-2-oxo-2,9-dihydro-10-oxa-1,3,9-triaza-anthracen-3-yl)-acetic acid tert-butyl ester

: 476667-26-2
C₃₅H₃₆N₆O₉

Guidance literature:: With Ph₂PC₆H₄-polymer; diethylazodicarboxylate; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1021/ol026815p

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: 476667-26-2
C₃₅H₃₆N₆O₉

Guidance literature:: Multi-step reaction with 5 steps

1.1: 85 percent / K₂CO₃ / dimethylformamide / 21 h / 20 °C

2.1: POCl₃; TEA / acetonitrile / 0.5 h / 0 °C

2.2: 90 percent / acetonitrile / 21 h / 20 °C

3.1: 80 percent / DBU / acetonitrile / 20 h / 20 °C

4.1: 76 percent / KF / ethanol / 20 h / Heating

5.1: 39 percent / DEAD; Ph₂PC₆H₄-polymer / CH₂Cl₂ / 4 h / 20 °C

With potassium fluoride; Ph₂PC₆H₄-polymer; TEA; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; diethylazodicarboxylate; trichlorophosphate; In ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 5.1: Mitsunobu alkylation;
DOI:10.1021/ol026815p

Reference yield:

: 601-89-8
2-nitroresorcinol

: 476667-26-2
C₃₅H₃₆N₆O₉

Guidance literature:: Multi-step reaction with 4 steps

1.1: 70 percent / sodium dithionite / ethanol; H₂O / 0.5 h / 20 °C

2.1: Ph₃P; CCl₄ / CH₂Cl₂ / 3 h / Heating

2.2: 12 percent / DBU / CH₂Cl₂ / 13 h / 20 °C

3.1: 76 percent / KF / ethanol / 20 h / Heating

4.1: 39 percent / DEAD; Ph₂PC₆H₄-polymer / CH₂Cl₂ / 4 h / 20 °C

With tetrachloromethane; potassium fluoride; sodium dithionite; Ph₂PC₆H₄-polymer; triphenylphosphine; diethylazodicarboxylate; In ethanol; dichloromethane; water; 4.1: Mitsunobu alkylation;
DOI:10.1021/ol026815p