1,2,9,13b-tetrahydro-3H-dibenzimidazo<1,5-a>azepine-3-thione

Base Information

Chemical Name:1,2,9,13b-tetrahydro-3H-dibenzimidazo<1,5-a>azepine-3-thione
CAS No.:80012-85-7
Molecular Formula:C₁₆H₁₄N₂S
Molecular Weight:266.367
Hs Code.:

1,2,9,13b-tetrahydro-3H-dibenz<c,f>imidazo<1,5-a>azepine-3-thione

Synonyms:1,2,9,13b-tetrahydro-3H-dibenzimidazo<1,5-a>azepine-3-thione

Suppliers and Price of 1,2,9,13b-tetrahydro-3H-dibenzimidazo<1,5-a>azepine-3-thione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1,2,9,13b-tetrahydro-3H-dibenzimidazo<1,5-a>azepine-3-thione

Chemical Property:

Purity/Quality:: 95%+ or 98%+ ^*data from raw suppliers

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Technology Process of 1,2,9,13b-tetrahydro-3H-dibenzimidazo<1,5-a>azepine-3-thione

There total 2 articles about 1,2,9,13b-tetrahydro-3H-dibenzimidazo<1,5-a>azepine-3-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 41218-84-2
6-aminomethyl-6,11-dihydro-5H-dibenzo[b,e]azepine

: 80012-85-7
1,2,9,13b-tetrahydro-3H-dibenzimidazo<1,5-a>azepine-3-thione

Guidance literature:: In toluene; at 60 ℃; for 1h;

Reference yield:

: 80012-69-7
11H-dibenzazepine-6-carbonitrile

: 80012-85-7
1,2,9,13b-tetrahydro-3H-dibenzimidazo<1,5-a>azepine-3-thione

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 100percent sulfuric acid, lithium aluminium hydride / tetrahydrofuran / 2 h / below 40 deg C

2: toluene / 1 h / 60 °C

With lithium aluminium tetrahydride; sulfuric acid; In tetrahydrofuran; toluene;