(E)-2-(3,3-Diphenylprop-2-enylidene)-1-hydroxymethyl-1-methylcyclopentane

Base Information

Chemical Name:(E)-2-(3,3-Diphenylprop-2-enylidene)-1-hydroxymethyl-1-methylcyclopentane
CAS No.:361447-35-0
Molecular Formula:C₂₂H₂₄O
Molecular Weight:304.432
Hs Code.:

Synonyms:(E)-2-(3,3-Diphenylprop-2-enylidene)-1-hydroxymethyl-1-methylcyclopentane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-2-(3,3-Diphenylprop-2-enylidene)-1-hydroxymethyl-1-methylcyclopentane

Chemical Property:

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Technology Process of (E)-2-(3,3-Diphenylprop-2-enylidene)-1-hydroxymethyl-1-methylcyclopentane

There total 3 articles about (E)-2-(3,3-Diphenylprop-2-enylidene)-1-hydroxymethyl-1-methylcyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 361447-34-9
Ethyl (E)-2-(3,3-diphenylprop-2-enylidene)-1-methylcyclopentanecarboxylate

: 361447-35-0
(E)-2-(3,3-Diphenylprop-2-enylidene)-1-hydroxymethyl-1-methylcyclopentane

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 20 ℃; for 1h;
DOI:10.1055/s-2001-15059

Reference yield:

: 27329-60-8
diethyl (diphenylmethyl)phosphonate

: 361447-35-0
(E)-2-(3,3-Diphenylprop-2-enylidene)-1-hydroxymethyl-1-methylcyclopentane

Guidance literature:: Multi-step reaction with 2 steps

1.1: BuLi / 1,2-dimethoxy-ethane; hexane / 1 h / 0 °C

1.2: 79 percent / hexane; 1,2-dimethoxy-ethane / 3 h / 0 °C

2.1: 89 percent / LiAlH₄ / diethyl ether / 1 h / 20 °C

With lithium aluminium tetrahydride; n-butyllithium; In 1,2-dimethoxyethane; diethyl ether; hexane;
DOI:10.1055/s-2001-15059

Reference yield:

: Ethyl 2-formylmethylidene-1-methylcyclopentanecarboxylate

: 361447-35-0
(E)-2-(3,3-Diphenylprop-2-enylidene)-1-hydroxymethyl-1-methylcyclopentane

Guidance literature:: Multi-step reaction with 2 steps

1.1: BuLi / 1,2-dimethoxy-ethane; hexane / 1 h / 0 °C

1.2: 79 percent / hexane; 1,2-dimethoxy-ethane / 3 h / 0 °C

2.1: 89 percent / LiAlH₄ / diethyl ether / 1 h / 20 °C

With lithium aluminium tetrahydride; n-butyllithium; In 1,2-dimethoxyethane; diethyl ether; hexane;
DOI:10.1055/s-2001-15059