C₁₇H₂₈O₃Si

Base Information

Chemical Name:C₁₇H₂₈O₃Si
CAS No.:1332745-49-9
Molecular Formula:C₁₇H₂₈O₃Si
Molecular Weight:308.493
Hs Code.:

C<sub>17</sub>H<sub>28</sub>O<sub>3</sub>Si

Synonyms:C₁₇H₂₈O₃Si

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Chemical Property of C₁₇H₂₈O₃Si

Chemical Property:

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Technology Process of C₁₇H₂₈O₃Si

There total 1 articles about C₁₇H₂₈O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69361-41-7
4-bromo-1-trimethylsilylbut-1-yne

: 118653-39-7
methyl 3,3-dimethyl-6-oxocyclohex-1-ene-1-carboxylate

: 1332745-49-9
C₁₇H₂₈O₃Si

Guidance literature:: 4-bromo-1-trimethylsilylbut-1-yne; With iodine; magnesium; In tetrahydrofuran; at 20 ℃; for 0.5h; Reflux; Inert atmosphere;

methyl 3,3-dimethyl-6-oxocyclohex-1-ene-1-carboxylate; With chloro-trimethyl-silane; copper(I) bromide dimethylsulfide complex; In tetrahydrofuran; at -78 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja206837j

Reference yield:

: 1332745-49-9
C₁₇H₂₈O₃Si

: 1-[(trimethylsilyl)ethynyl]-1,2-benziodoxol-3(1H)-one

: C₁₉H₂₈O₃Si

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at -78 - -40 ℃; for 4h; Inert atmosphere;

Reference yield:

: 1332745-49-9
C₁₇H₂₈O₃Si

: C₁₅H₂₀O₂

Guidance literature:: Multi-step reaction with 4 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / -78 - -40 °C / Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / -40 - 20 °C / Inert atmosphere

3: potassium hydroxide / tetrahydrofuran; methanol; water / 6 h / Inert atmosphere; Reflux

4: 2,2,6,6-tetramethyl-piperidine-N-oxyl; I,I-bis(acetoxy)iodobenzene / dichloromethane / 12 h / 20 °C / Inert atmosphere

With 2,2,6,6-tetramethyl-piperidine-N-oxyl; lithium aluminium tetrahydride; tetrabutyl ammonium fluoride; I,I-bis(acetoxy)iodobenzene; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1021/ja206837j