C₄₃H₅₆O₇

Base Information

Chemical Name:C₄₃H₅₆O₇
CAS No.:1449419-33-3
Molecular Formula:C₄₃H₅₆O₇
Molecular Weight:684.913
Hs Code.:

C<sub>43</sub>H<sub>56</sub>O<sub>7</sub>

Synonyms:C₄₃H₅₆O₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₃H₅₆O₇

Chemical Property:

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Technology Process of C₄₃H₅₆O₇

There total 5 articles about C₄₃H₅₆O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1449419-27-5
C₅₁H₆₄O₈

: 1449419-33-3
C₄₃H₅₆O₇

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; at 20 ℃; for 1h;
DOI:10.1016/j.tet.2013.02.008

Reference yield:

: 1449419-19-5
C₁₆H₂₄O₃S₂

: 1449419-33-3
C₄₃H₅₆O₇

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

1.2: 21.5 h / 0 - 20 °C

2.1: sodium hydrogencarbonate; methyl iodide / acetonitrile; water / 19 h / 20 °C

3.1: sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium chlorite / tetrahydrofuran; water; tert-butyl alcohol / 0.5 h / 4 °C

4.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 3 h / 20 °C

4.2: 1.5 h / 50 °C

5.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 1 h / 20 °C

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; 2,4,6-trichlorobenzoyl chloride; sodium hydride; sodium hydrogencarbonate; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; methyl iodide; In tetrahydrofuran; dichloromethane; water; toluene; acetonitrile; mineral oil; tert-butyl alcohol; 4.1: |Yamaguchi Lactonization / 4.2: |Yamaguchi Lactonization;
DOI:10.1016/j.tet.2013.02.008

Reference yield:

: 1449419-21-9
C₂₃H₃₀O₃S₂

: 1449419-33-3
C₄₃H₅₆O₇

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydrogencarbonate; methyl iodide / acetonitrile; water / 19 h / 20 °C

2.1: sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium chlorite / tetrahydrofuran; water; tert-butyl alcohol / 0.5 h / 4 °C

3.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 3 h / 20 °C

3.2: 1.5 h / 50 °C

4.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 1 h / 20 °C

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; 2,4,6-trichlorobenzoyl chloride; sodium hydrogencarbonate; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; methyl iodide; In tetrahydrofuran; dichloromethane; water; toluene; acetonitrile; tert-butyl alcohol; 3.1: |Yamaguchi Lactonization / 3.2: |Yamaguchi Lactonization;
DOI:10.1016/j.tet.2013.02.008