benzyl 3-benzamido-2,3,6-trideoxy-2-fluoro-α-D-arabino-hex-5-enopyranoside

Base Information

Chemical Name:benzyl 3-benzamido-2,3,6-trideoxy-2-fluoro-α-D-arabino-hex-5-enopyranoside
CAS No.:99388-58-6
Molecular Formula:C₂₀H₂₀FNO₄
Molecular Weight:357.382
Hs Code.:

Synonyms:benzyl 3-benzamido-2,3,6-trideoxy-2-fluoro-α-D-arabino-hex-5-enopyranoside

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Chemical Property of benzyl 3-benzamido-2,3,6-trideoxy-2-fluoro-α-D-arabino-hex-5-enopyranoside

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Technology Process of benzyl 3-benzamido-2,3,6-trideoxy-2-fluoro-α-D-arabino-hex-5-enopyranoside

There total 6 articles about benzyl 3-benzamido-2,3,6-trideoxy-2-fluoro-α-D-arabino-hex-5-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 99388-57-5
benzyl 3-benzamido-2,3,6-trideoxy-2-fluoro-6-iodo-α-D-altropyranoside

: 99388-58-6
benzyl 3-benzamido-2,3,6-trideoxy-2-fluoro-α-D-arabino-hex-5-enopyranoside

Guidance literature:: With silver fluoride; In pyridine; for 24h; Ambient temperature; dark;
DOI:10.1016/0008-6215(85)85048-5

Reference yield:

: 4710-91-2,13347-86-9,19374-63-1,144789-62-8
benzyl 2-benzamido-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

: 99388-58-6
benzyl 3-benzamido-2,3,6-trideoxy-2-fluoro-α-D-arabino-hex-5-enopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 75 percent / pyridine / 72 h / Ambient temperature

2: 40 percent / tetrabutylammonium fluoride / hexamethylphosphoric acid triamide / 6 h / 85 °C

3: 99 percent / hydrochloric acid / ethanol / 12 h / Ambient temperature

4: 76 percent / pyridine / 1.5 h / Ambient temperature

5: 99 percent / sodium iodide / butan-2-one / 15 h / Heating

6: 53 percent / silver fluoride / pyridine / 24 h / Ambient temperature; dark

With pyridine; hydrogenchloride; tetrabutyl ammonium fluoride; silver fluoride; sodium iodide; In pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; butanone;
DOI:10.1016/0008-6215(85)85048-5

Reference yield:

: 99388-54-2
benzyl 3-benzamido-2,3-dideoxy-2-fluoro-α-D-altropyranoside

: 99388-58-6
benzyl 3-benzamido-2,3,6-trideoxy-2-fluoro-α-D-arabino-hex-5-enopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / pyridine / 1.5 h / Ambient temperature

2: 99 percent / sodium iodide / butan-2-one / 15 h / Heating

3: 53 percent / silver fluoride / pyridine / 24 h / Ambient temperature; dark

With pyridine; silver fluoride; sodium iodide; In pyridine; butanone;
DOI:10.1016/0008-6215(85)85048-5