C₁₂H₁₅N₃O₄

Base Information

Chemical Name:C₁₂H₁₅N₃O₄
CAS No.:1428631-95-1
Molecular Formula:C₁₂H₁₅N₃O₄
Molecular Weight:265.269
Hs Code.:

C<sub>12</sub>H<sub>15</sub>N<sub>3</sub>O<sub>4</sub>

Synonyms:C₁₂H₁₅N₃O₄

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Chemical Property of C₁₂H₁₅N₃O₄

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Technology Process of C₁₂H₁₅N₃O₄

There total 5 articles about C₁₂H₁₅N₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: C₂₈H₂₇N₃O₆

: 1428631-95-1
C₁₂H₁₅N₃O₄

Guidance literature:: With sodium methylate; In methanol; dichloromethane; at 5 - 20 ℃; for 0.833333h;
DOI:10.1021/ja312148q

Reference yield:

: 1428631-84-8
C₂₈H₂₉NO₆

: 1428631-95-1
C₁₂H₁₅N₃O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride / tetrahydrofuran; water / 0.25 h / 0 °C

1.2: 0.67 h / 0 °C

1.3: 2.6 h / 0 - 20 °C

2.1: copper(l) iodide; sodium azide; N,N`-dimethylethylenediamine; sodium L-ascorbate / water; ethanol / 0.75 h / 90 °C

3.1: sodium methylate / dichloromethane; methanol / 0.83 h / 5 - 20 °C

With hydrogenchloride; copper(l) iodide; sodium azide; sodium methylate; sodium L-ascorbate; N,N`-dimethylethylenediamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; 1.2: |Sandmeyer Reaction / 1.3: |Sandmeyer Reaction;
DOI:10.1021/ja312148q

Reference yield:

: 1364927-25-2
C₂₀H₂₃NO₆

: 1428631-95-1
C₁₂H₁₅N₃O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine / 15 h / 20 °C / Inert atmosphere

2.1: triethylamine; palladium 10% on activated carbon; hydrogen / ethyl acetate / 1 h / 20 °C

3.1: hydrogenchloride / tetrahydrofuran; water / 0.25 h / 0 °C

3.2: 0.67 h / 0 °C

3.3: 2.6 h / 0 - 20 °C

4.1: copper(l) iodide; sodium azide; N,N`-dimethylethylenediamine; sodium L-ascorbate / water; ethanol / 0.75 h / 90 °C

5.1: sodium methylate / dichloromethane; methanol / 0.83 h / 5 - 20 °C

With pyridine; hydrogenchloride; copper(l) iodide; sodium azide; palladium 10% on activated carbon; hydrogen; sodium methylate; sodium L-ascorbate; triethylamine; N,N`-dimethylethylenediamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; ethyl acetate; 3.2: |Sandmeyer Reaction / 3.3: |Sandmeyer Reaction;
DOI:10.1021/ja312148q