C₃₉H₆₁NO₁₀Si

Base Information

Chemical Name:C₃₉H₆₁NO₁₀Si
CAS No.:1199945-08-8
Molecular Formula:C₃₉H₆₁NO₁₀Si
Molecular Weight:732
Hs Code.:

C<sub>39</sub>H<sub>61</sub>NO<sub>10</sub>Si

Synonyms:C₃₉H₆₁NO₁₀Si

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Chemical Property of C₃₉H₆₁NO₁₀Si

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Technology Process of C₃₉H₆₁NO₁₀Si

There total 10 articles about C₃₉H₆₁NO₁₀Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1148112-29-1
C₄₀H₆₃NO₈Si

: 1199945-08-8
C₃₉H₆₁NO₁₀Si

Guidance literature:: With osmium(VIII) oxide; sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1002/anie.200805334

Reference yield:

: C₃₉H₆₃NO₅Si

: 1199945-08-8
C₃₉H₆₁NO₁₀Si

Guidance literature:: With Oxone; osmium(VIII) oxide; sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 20 ℃; for 6h;

Reference yield:

: 1148112-25-7
C₂₃H₃₄O₄Si

: 1199945-08-8
C₃₉H₆₁NO₁₀Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: triethylamine; (S)-Ph,(R)-tBu-CuCl₂(C₅H₃NBrCHNCH(tBu)C₃H₃NO(Ph)) / tetrahydrofuran / 0.5 h / 20 °C

2.1: triethylamine; methanesulfonyl chloride / 0.5 h / -78 °C

2.2: 6 h / 20 °C

3.1: methanol; potassium carbonate / 2 h / 20 °C

4.1: triethylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 1 h / 0 °C

5.1: tetrahydrofuran / 16 h / -78 °C

6.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; toluene / 8 h / 0 °C

7.1: silver trifluoromethanesulfonate / dichloromethane; toluene / 4 h / 0 - 20 °C / Molecular sieve

8.1: ozone / methanol / -78 °C

8.2: 0.17 h / -78 - 0 °C

9.1: sodium hydrogencarbonate; osmium(VIII) oxide; Oxone / N,N-dimethyl-formamide / 6 h / 20 °C

With methanol; Oxone; osmium(VIII) oxide; (S)-Ph,(R)-tBu-CuCl₂(C₅H₃NBrCHNCH(tBu)C₃H₃NO(Ph)); silver trifluoromethanesulfonate; sulfur trioxide pyridine complex; sodium hydrogencarbonate; potassium carbonate; ozone; methanesulfonyl chloride; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;