C₅₄H₉₂O₉Si₃

Base Information

Chemical Name:C₅₄H₉₂O₉Si₃
CAS No.:440643-02-7
Molecular Formula:C₅₄H₉₂O₉Si₃
Molecular Weight:969.576
Hs Code.:

C<sub>54</sub>H<sub>92</sub>O<sub>9</sub>Si<sub>3</sub>

Synonyms:C₅₄H₉₂O₉Si₃

Suppliers and Price of C₅₄H₉₂O₉Si₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₄H₉₂O₉Si₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₄H₉₂O₉Si₃

There total 19 articles about C₅₄H₉₂O₉Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 440643-03-8
C₆₂H₁₀₀O₁₀Si₃

: 440643-02-7
C₅₄H₉₂O₉Si₃

Guidance literature:: With hydrogen; palladium dihydroxide; In ethanol;
DOI:10.1016/S0040-4020(02)00050-9

Reference yield:

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 440643-02-7
C₅₄H₉₂O₉Si₃

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / pyridine; DMAP / 15 h

2: aq. LiOH / tetrahydrofuran; 2-methyl-propan-2-ol / 2 h / 20 °C

3: 34.2 mg / benzene; methanol; hexane / 0.25 h / 20 °C

With pyridine; dmap; lithium hydroxide; In tetrahydrofuran; methanol; hexane; tert-butyl alcohol; benzene;
DOI:10.1016/S0040-4020(02)00050-9

Reference yield:

: 214483-93-9
(3E,5S,9S,10E)-5,9-dimethyl-1,13-bis(benzyloxy)-3,10-tridecadien-7-one

: 440643-02-7
C₅₄H₉₂O₉Si₃

Guidance literature:: Multi-step reaction with 14 steps

1.1: AD-mix-α / 2-methyl-propan-2-ol; H2O / 24 h / 0 °C

2.1: CSA / benzene; methanol / 32 h

2.2: H₂ / Pd(OH)2 / ethanol / 12 h / 20 °C / 760 Torr

3.1: 98 percent / TFA / methanol / 0.83 h / Heating

4.1: 75 percent / NMO; 4 Angstroem molecular sieves; TPAP / 2-methyl-propan-2-ol; acetonitrile / 20 °C

5.1: pyridine / tetrahydrofuran; toluene / 0.75 h / -78 - 20 °C

5.2: 9-BBN / tetrahydrofuran; toluene / 0.5 h / 20 °C

5.3: 40 percent / NaBO₃*4H₂O / tetrahydrofuran; toluene / 2 h

6.1: Dess-Martin periodinane reagent / CH₂Cl₂ / 2.5 h / 20 °C

7.1: 77 percent / TiCl₄ / CH₂Cl₂ / 0.33 h / -78 °C

8.1: 91 percent / pyridine; DMAP / 27 h / 20 °C

9.1: 99 percent / IBr / toluene; CH₂Cl₂ / 3 h / -80 °C

10.1: 90 percent / aq. LiOH / 1,2-dimethoxy-ethane / 13 h / 60 °C

11.1: 90 percent / pyridine; DMAP / CH₂Cl₂ / 16 h / 20 °C

12.1: 99 percent / pyridine; DMAP / 15 h

13.1: aq. LiOH / tetrahydrofuran; 2-methyl-propan-2-ol / 2 h / 20 °C

14.1: 34.2 mg / benzene; methanol; hexane / 0.25 h / 20 °C

With pyridine; dmap; lithium hydroxide; AD-mix-α; N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 A molecular sieve; camphor-10-sulfonic acid; iodine(I) bromide; titanium tetrachloride; Dess-Martin periodane; trifluoroacetic acid; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; hexane; dichloromethane; water; toluene; acetonitrile; tert-butyl alcohol; benzene;
DOI:10.1016/S0040-4020(02)00050-9