Technology Process of C30H32N2O6
There total 7 articles about C30H32N2O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
N,N-dimethyl-formamide;
at 0 - 20 ℃;
for 3.5h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium iodide; potassium carbonate / N,N-dimethyl-formamide / 1.5 h / 70 °C / Inert atmosphere
2: sodium hydroxide; water / methanol; thiophene / 1.5 h / 70 °C / Inert atmosphere
3: tetrahydrofuran / 20 °C / Inert atmosphere
4: Dess-Martin periodane / dichloromethane / 2 h / 0 °C / Inert atmosphere
5: aminosulfonic acid; sodium chlorite / 1,4-dioxane; water / 0.5 h / 0 °C / Inert atmosphere
6: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 3.5 h / 0 - 20 °C / Inert atmosphere
With
sodium chlorite; aminosulfonic acid; water; potassium carbonate; benzotriazol-1-ol; Dess-Martin periodane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium iodide; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; thiophene; methanol; dichloromethane; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydroxide; water / methanol; thiophene / 1.5 h / 70 °C / Inert atmosphere
2: tetrahydrofuran / 20 °C / Inert atmosphere
3: Dess-Martin periodane / dichloromethane / 2 h / 0 °C / Inert atmosphere
4: aminosulfonic acid; sodium chlorite / 1,4-dioxane; water / 0.5 h / 0 °C / Inert atmosphere
5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 3.5 h / 0 - 20 °C / Inert atmosphere
With
sodium chlorite; aminosulfonic acid; water; benzotriazol-1-ol; Dess-Martin periodane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; thiophene; methanol; dichloromethane; water; N,N-dimethyl-formamide;