N-(3,5-Di-tert-butylphenyl)-4-methylbenzenesulfenamide

Base Information

• Chemical Name: N-(3,5-Di-tert-butylphenyl)-4-methylbenzenesulfenamide
• CAS No.: 74282-60-3
• Molecular Formula: C₂₁H₂₉NS
• Molecular Weight: 327.534
• Mol file: 74282-60-3.mol

Synonyms:N-(3,5-Di-tert-butylphenyl)-4-methylbenzenesulfenamide

Chemical Property of N-(3,5-Di-tert-butylphenyl)-4-methylbenzenesulfenamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(3,5-Di-tert-butylphenyl)-4-methylbenzenesulfenamide

There total 1 articles about N-(3,5-Di-tert-butylphenyl)-4-methylbenzenesulfenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

p-methylbenzenesulfenyl chloride (933-00-6) + 3,5-di-tert-butylaniline (2380-36-1) → N-(3,5-Di-tert-butylphenyl)-4-methylbenzenesulfenamide (74282-60-3)

Guidance literature:

With triethylamine; In diethyl ether; at 0 - 5 ℃; for 1h;

DOI:10.1021/jo01307a028

Reference yield: 54.0%

N-(3,5-Di-tert-butylphenyl)-4-methylbenzenesulfenamide (74282-60-3) → N,N'-Bis(3,5-di-tert-butylphenyl)-N,N'-bis<(4-methylphenyl)thio>hydrazine (74282-73-8)

Guidance literature:

With potassium carbonate; lead dioxide; In benzene; for 0.25h; Ambient temperature;

DOI:10.1021/jo01307a028

Reference yield:

N-(3,5-Di-tert-butylphenyl)-4-methylbenzenesulfenamide (74282-60-3) → N-(4-Methylphenylthio)-3,5-di-tert-butylphenylaminyl (74282-68-1)

Guidance literature:

With potassium carbonate; lead dioxide; In benzene; Ambient temperature;

DOI:10.1021/jo01307a028

upstream raw materials:

p-methylbenzenesulfenyl chloride

3,5-di-tert-butylaniline

Downstream raw materials:

N-(4-Methylphenylthio)-3,5-di-tert-butylphenylaminyl

N,N'-Bis(3,5-di-tert-butylphenyl)-N,N'-bis<(4-methylphenyl)thio>hydrazine