C₃₀H₄₂N₁₀

Base Information

• Chemical Name: C₃₀H₄₂N₁₀
• CAS No.: 1415583-65-1
• Molecular Formula: C₃₀H₄₂N₁₀
• Molecular Weight: 542.73
• Mol file: 1415583-65-1.mol

Synonyms:C₃₀H₄₂N₁₀

Chemical Property of C₃₀H₄₂N₁₀

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₄₂N₁₀

There total 2 articles about C₃₀H₄₂N₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzamidine monohydrochloride (1670-14-0) → C30H42N10 (1415583-65-1)

Guidance literature:

Multi-step reaction with 4 steps

1.1: sodium methylate / methanol / 2 h / 55 °C

1.2: 0.5 h

2.1: hydrogenchloride; sodium nitrite / water

2.2: 0.5 h

3.1: N-ethyl-N,N-diisopropylamine; trichlorophosphate / 1 h / Reflux

4.1: N-ethyl-N,N-diisopropylamine / iso-butanol / 2 h / 115 °C

With hydrogenchloride; sodium methylate; N-ethyl-N,N-diisopropylamine; sodium nitrite; trichlorophosphate; In methanol; water; iso-butanol;

Reference yield:

2-Phenyl-4,6-dihydroxy-pyrimidine (13566-71-7) → C30H42N10 (1415583-65-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: hydrogenchloride; sodium nitrite / water

1.2: 0.5 h

2.1: N-ethyl-N,N-diisopropylamine; trichlorophosphate / 1 h / Reflux

3.1: N-ethyl-N,N-diisopropylamine / iso-butanol / 2 h / 115 °C

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; sodium nitrite; trichlorophosphate; In water; iso-butanol;

Reference yield:

C30H42N10 (1415583-65-1) → C24H39N9 (1415583-66-2)

Guidance literature:

With methanol; ammonium formate; palladium-on-charcoal; In tetrahydrofuran; water; at 55 ℃; for 0.25h; Reflux;

upstream raw materials:

benzamidine monohydrochloride

2-Phenyl-4,6-dihydroxy-pyrimidine

Downstream raw materials:

C₂₄H₃₉N₉

C₂₅H₃₇N₉