(2R,3S,4S)-2-(benzylamino)-4-<valyl>amino>-3-hydoxy-5-phenylpentanoic acid ethyl ester

Base Information

Chemical Name:(2R,3S,4S)-2-(benzylamino)-4-<valyl>amino>-3-hydoxy-5-phenylpentanoic acid ethyl ester
CAS No.:161510-65-2
Molecular Formula:C₃₃H₄₁N₃O₆
Molecular Weight:575.705
Hs Code.:

(2R,3S,4S)-2-(benzylamino)-4-<<N-<(benzyloxy)carbonyl>valyl>amino>-3-hydoxy-5-phenylpentanoic acid ethyl ester

Synonyms:(2R,3S,4S)-2-(benzylamino)-4-<valyl>amino>-3-hydoxy-5-phenylpentanoic acid ethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3S,4S)-2-(benzylamino)-4-<valyl>amino>-3-hydoxy-5-phenylpentanoic acid ethyl ester

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Technology Process of (2R,3S,4S)-2-(benzylamino)-4-<valyl>amino>-3-hydoxy-5-phenylpentanoic acid ethyl ester

There total 1 articles about (2R,3S,4S)-2-(benzylamino)-4-<valyl>amino>-3-hydoxy-5-phenylpentanoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: (2S/R,3R,S,4S)-4-<valyl>amino>-2,3-epoxy-5-phenylpentanoic acid ethyl ester

: 100-46-9
benzylamine

: 161510-65-2
(2R,3S,4S)-2-(benzylamino)-4-<valyl>amino>-3-hydoxy-5-phenylpentanoic acid ethyl ester

Guidance literature:: In ethanol; at 60 ℃; for 48h;
DOI:10.1021/jm00045a013

Reference yield: 89.0%

: 161510-65-2
(2R,3S,4S)-2-(benzylamino)-4-<valyl>amino>-3-hydoxy-5-phenylpentanoic acid ethyl ester

: 161510-67-4
(2R,3S,4S)-2-(benzylamino)-4-<valyl>amino>-3-hydoxy-5-phenylpentanoic acid

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; for 10h; Ambient temperature;
DOI:10.1021/jm00045a013

Reference yield:

: 161510-65-2
(2R,3S,4S)-2-(benzylamino)-4-<valyl>amino>-3-hydoxy-5-phenylpentanoic acid ethyl ester

: 161510-57-2
SDZ 282312

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / 1N aq. NaOH / tetrahydrofuran / 10 h / Ambient temperature

2: 1-hydroxybenzotriazole, EDC*HCl / dimethylformamide / Ambient temperature

With sodium hydroxide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm00045a013