(+/-)-1-[(1S,5R)-2-methyl-5-(1-methylvinyl)cyclohex-2-enyl]-4-methylbenzene

Base Information

Chemical Name:(+/-)-1-[(1S,5R)-2-methyl-5-(1-methylvinyl)cyclohex-2-enyl]-4-methylbenzene
CAS No.:376353-55-8
Molecular Formula:C₁₇H₂₂
Molecular Weight:226.362
Hs Code.:

Synonyms:(+/-)-1-[(1S,5R)-2-methyl-5-(1-methylvinyl)cyclohex-2-enyl]-4-methylbenzene

Suppliers and Price of (+/-)-1-[(1S,5R)-2-methyl-5-(1-methylvinyl)cyclohex-2-enyl]-4-methylbenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-1-[(1S,5R)-2-methyl-5-(1-methylvinyl)cyclohex-2-enyl]-4-methylbenzene

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Technology Process of (+/-)-1-[(1S,5R)-2-methyl-5-(1-methylvinyl)cyclohex-2-enyl]-4-methylbenzene

There total 3 articles about (+/-)-1-[(1S,5R)-2-methyl-5-(1-methylvinyl)cyclohex-2-enyl]-4-methylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 18412-57-2
p-tolyltriethoxysilane

: 121156-22-7
(+)-(R,R)-cis-carveolbenzoate

: 376353-55-8
(+/-)-1-[(1S,5R)-2-methyl-5-(1-methylvinyl)cyclohex-2-enyl]-4-methylbenzene

Guidance literature:: With tetrabutyl ammonium fluoride; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; at 60 ℃; for 48h;
DOI:10.1021/jo010627f

Reference yield: 69.0%

: 106-38-7
para-bromotoluene

: 121156-22-7
(+)-(R,R)-cis-carveolbenzoate

: 376353-55-8
(+/-)-1-[(1S,5R)-2-methyl-5-(1-methylvinyl)cyclohex-2-enyl]-4-methylbenzene

Guidance literature:: para-bromotoluene; With tert.-butyl lithium; In tetrahydrofuran; pentane; at 0 ℃; for 1h;

With indium(III) chloride; In tetrahydrofuran; pentane; at -78 - 20 ℃;

(+)-(R,R)-cis-carveolbenzoate; With triphenylphosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In tetrahydrofuran; pentane; at 55 ℃; for 2h;
DOI:10.1021/jo0357162

Reference yield:

: 106-38-7
para-bromotoluene

: 119905-76-9
(1S,5R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-2-en-1-yl benzoate

: 376353-55-8
(+/-)-1-[(1S,5R)-2-methyl-5-(1-methylvinyl)cyclohex-2-enyl]-4-methylbenzene

: (+/-)-1-[(1R,5R)-2-methyl-5-(1-methylvinyl)cyclohex-2-enyl]-4-methylbenzene

Guidance literature:: para-bromotoluene; With tert.-butyl lithium; In diethyl ether; pentane; at 0 ℃; for 1h;

With indium(III) chloride; In diethyl ether; pentane; at -78 - 20 ℃;

(1S,5R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-2-en-1-yl benzoate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In diethyl ether; N,N-dimethyl-formamide; pentane; at 55 ℃; for 4h;
DOI:10.1021/jo0357162