N,N',N-tris[2,3-di(benzyloxy)benzoyl-glycinyl]cyclotri-Dseryl trilactone

Base Information

• Chemical Name: N,N',N-tris[2,3-di(benzyloxy)benzoyl-glycinyl]cyclotri-Dseryl trilactone
• CAS No.: 1186383-38-9
• Molecular Formula: C₇₈H₇₂N₆O₁₈
• Molecular Weight: 1381.46
• Mol file: 1186383-38-9.mol

Synonyms:N,N',N-tris[2,3-di(benzyloxy)benzoyl-glycinyl]cyclotri-Dseryl trilactone

Chemical Property of N,N',N-tris[2,3-di(benzyloxy)benzoyl-glycinyl]cyclotri-Dseryl trilactone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N',N-tris[2,3-di(benzyloxy)benzoyl-glycinyl]cyclotri-Dseryl trilactone

There total 1 articles about N,N',N-tris[2,3-di(benzyloxy)benzoyl-glycinyl]cyclotri-Dseryl trilactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

tris(N-hydrochloride-D-serine) trilactone (75363-10-9) + 2,3-bis(benzyloxy)glycinylfluoride benzoylamide (416843-20-4) → N,N',N-tris[2,3-di(benzyloxy)benzoyl-glycinyl]cyclotri-Dseryl trilactone (1186383-38-9)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃; Cooling with ice;

DOI:10.1021/ja903051q

Reference yield: 88.0%

N,N',N-tris[2,3-di(benzyloxy)benzoyl-glycinyl]cyclotri-Dseryl trilactone (1186383-38-9) → N,N',N-tris[2,3-dihydroxybenzoyl-glycinyl]cyclotri-Dseryl trilactone (921608-54-0)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethanol; ethyl acetate; at 20 ℃; for 24h; under 760.051 Torr;

DOI:10.1021/ja903051q

upstream raw materials:

tris(N-hydrochloride-D-serine) trilactone

2,3-bis(benzyloxy)glycinylfluoride benzoylamide

Downstream raw materials:

N,N',N-tris[2,3-dihydroxybenzoyl-glycinyl]cyclotri-Dseryl trilactone