4-(2-benzyloxy-4-hydroxyphenyl)-3-[3-(tert-butyldimethylsilanyloxy)-3-(4-fluorophenyl)propyl]-1-(4-fluorophenyl)azetidin-2-one

Base Information

• Chemical Name: 4-(2-benzyloxy-4-hydroxyphenyl)-3-[3-(tert-butyldimethylsilanyloxy)-3-(4-fluorophenyl)propyl]-1-(4-fluorophenyl)azetidin-2-one
• CAS No.: 937798-31-7
• Molecular Formula: C₃₇H₄₁F₂NO₄Si
• Molecular Weight: 629.819

Synonyms:4-(2-benzyloxy-4-hydroxyphenyl)-3-[3-(tert-butyldimethylsilanyloxy)-3-(4-fluorophenyl)propyl]-1-(4-fluorophenyl)azetidin-2-one

Chemical Property of 4-(2-benzyloxy-4-hydroxyphenyl)-3-[3-(tert-butyldimethylsilanyloxy)-3-(4-fluorophenyl)propyl]-1-(4-fluorophenyl)azetidin-2-one

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Technology Process of 4-(2-benzyloxy-4-hydroxyphenyl)-3-[3-(tert-butyldimethylsilanyloxy)-3-(4-fluorophenyl)propyl]-1-(4-fluorophenyl)azetidin-2-one

There total 1 articles about 4-(2-benzyloxy-4-hydroxyphenyl)-3-[3-(tert-butyldimethylsilanyloxy)-3-(4-fluorophenyl)propyl]-1-(4-fluorophenyl)azetidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C44H47F2NO4Si (937798-30-6) → 3-[3-(tert-butyldimethylsilanyloxy)-3-(4-fluorophenyl)propyl]-4-(2,4-dihydroxyphenyl)-1-(4-fluorophenyl)azetidin-2-one (937798-32-8) + 4-(4-benzyloxy-2-hydroxyphenyl)-3-[3-(tert-butyldimethylsilanyloxy)-3-(4-fluorophenyl)propyl]-1-(4-fluorophenyl)azetidin-2-one (937798-33-9) + 4-(2-benzyloxy-4-hydroxyphenyl)-3-[3-(tert-butyldimethylsilanyloxy)-3-(4-fluorophenyl)propyl]-1-(4-fluorophenyl)azetidin-2-one (937798-31-7)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In ethyl acetate; for 3h; under 3750.38 Torr;

Reference yield:

4-(2-benzyloxy-4-hydroxyphenyl)-3-[3-(tert-butyldimethylsilanyloxy)-3-(4-fluorophenyl)propyl]-1-(4-fluorophenyl)azetidin-2-one (937798-31-7) + 1,3,2-dioxathiane 2,2-dioxide (1073-05-8) → 3-{3-benzyloxy-4-[3-[3-(tert-butyldimethylsilanyloxy)-3-(4-fluorophenyl)propyl]-1-(4-fluorophenyl)-4-oxoazetidin-2-yl]phenoxy}propyl ammonium sulfate (937798-40-8)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

Reference yield:

(E)-1,4-dibromobutene (821-06-7) + 4-(2-benzyloxy-4-hydroxyphenyl)-3-[3-(tert-butyldimethylsilanyloxy)-3-(4-fluorophenyl)propyl]-1-(4-fluorophenyl)azetidin-2-one (937798-31-7) → 4-[2-benzyloxy-4-(4-bromobut-2-enyloxy)phenyl]-3-[3-(tert-butyldimethylsilanyloxy)-3-(4-fluorophenyl)propyl]-1-(4-fluorophenyl)azetidin-2-one

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide;

upstream raw materials:

C₄₄H₄₇F₂NO₄Si

Downstream raw materials:

3-{3-benzyloxy-4-[3-[3-(tert-butyldimethylsilanyloxy)-3-(4-fluorophenyl)propyl]-1-(4-fluorophenyl)-4-oxoazetidin-2-yl]phenoxy}propyl ammonium sulfate

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