2-(t-butoxycarbonyloxy)-5,8-bis<2-ethylamino>-1-hydroxy-9,10-anthracenedione

Base Information

• Chemical Name: 2-(t-butoxycarbonyloxy)-5,8-bis<2-ethylamino>-1-hydroxy-9,10-anthracenedione
• CAS No.: 87406-43-7
• Molecular Formula: C₇₅H₈₀N₄O₁₂
• Molecular Weight: 1229.48

Synonyms:2-(t-butoxycarbonyloxy)-5,8-bis<2-ethylamino>-1-hydroxy-9,10-anthracenedione

Chemical Property of 2-(t-butoxycarbonyloxy)-5,8-bis<2-ethylamino>-1-hydroxy-9,10-anthracenedione

Chemical Property:

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Technology Process of 2-(t-butoxycarbonyloxy)-5,8-bis<2-ethylamino>-1-hydroxy-9,10-anthracenedione

There total 1 articles about 2-(t-butoxycarbonyloxy)-5,8-bis<2-ethylamino>-1-hydroxy-9,10-anthracenedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

trityl chloride (76-83-5) + 2-(t-butoxycarbonyloxy)-5,8-bis<2-(N-t-butoxycarbonyl-2-hydroxyethylamino)ethylamino>-1-hydroxy-9,10-anthracenedione (87406-40-4) → 2-(t-butoxycarbonyloxy)-5,8-bis<2-ethylamino>-1-hydroxy-9,10-anthracenedione (87406-43-7)

Guidance literature:

With pyridine; at 60 ℃; for 17h;

DOI:10.1246/bcsj.56.1812

Reference yield: 94.0%

2-(t-butoxycarbonyloxy)-5,8-bis<2-ethylamino>-1-hydroxy-9,10-anthracenedione (87406-43-7) → 5,8-bis<2-ethylamino>-1,2-dihydroxy-9,10-anthracenedione (87406-42-6)

Guidance literature:

With potassium carbonate; In acetone; for 7h; Heating;

DOI:10.1246/bcsj.56.1812

Reference yield: 64.0%

dimethyl sulfate (77-78-1) + 2-(t-butoxycarbonyloxy)-5,8-bis<2-ethylamino>-1-hydroxy-9,10-anthracenedione (87406-43-7) → 1-(t-butoxycarbonyloxy)-5,8-bis<2-ethylamino>-2-methoxy-9,10-anthracenedione (87406-48-2)

Guidance literature:

With potassium carbonate; In acetone; for 6h; Heating;

DOI:10.1246/bcsj.56.1812

upstream raw materials:

trityl chloride

2-(t-butoxycarbonyloxy)-5,8-bis<2-(N-t-butoxycarbonyl-2-hydroxyethylamino)ethylamino>-1-hydroxy-9,10-anthracenedione

Downstream raw materials:

1-(t-butoxycarbonyloxy)-5,8-bis<2-ethylamino>-2-methoxy-9,10-anthracenedione

5,8-bis<2-ethylamino>-1,2-dihydroxy-9,10-anthracenedione

5,8-bis<2-ethylamino>-1-hydroxy-2-methoxy-9,10-anthracenedione

5,8-bis<2-ethylamino>-1,2-dimethoxy-9,10-anthracenedione

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