4-(5-amino-1H-[1,2,4]triazol-3-ylamino)-2-trifluoromethanesulfonylbenzonitrile

Base Information

Chemical Name:4-(5-amino-1H-[1,2,4]triazol-3-ylamino)-2-trifluoromethanesulfonylbenzonitrile
CAS No.:1533424-22-4
Molecular Formula:C₁₀H₇F₃N₆O₂S
Molecular Weight:332.266
Hs Code.:

Synonyms:4-(5-amino-1H-[1,2,4]triazol-3-ylamino)-2-trifluoromethanesulfonylbenzonitrile

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Chemical Property of 4-(5-amino-1H-[1,2,4]triazol-3-ylamino)-2-trifluoromethanesulfonylbenzonitrile

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Technology Process of 4-(5-amino-1H-[1,2,4]triazol-3-ylamino)-2-trifluoromethanesulfonylbenzonitrile

There total 6 articles about 4-(5-amino-1H-[1,2,4]triazol-3-ylamino)-2-trifluoromethanesulfonylbenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1533434-89-7
C₁₁H₇F₃N₄O₂S₂

: 1533424-22-4
4-(5-amino-1H-[1,2,4]triazol-3-ylamino)-2-trifluoromethanesulfonylbenzonitrile

Guidance literature:: With hydrazine; In ethanol; at 60 ℃; under 760.051 Torr; Inert atmosphere;

Reference yield:

: 1533425-08-9
N-(4-bromo-3-(trifluoromethylsulfonyl)phenyl)acetamide

: 1533424-22-4
4-(5-amino-1H-[1,2,4]triazol-3-ylamino)-2-trifluoromethanesulfonylbenzonitrile

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1-methyl-pyrrolidin-2-one / 1 h / 200 °C / 760.05 Torr / Microwave irradiation; Inert atmosphere

2.1: hydrogenchloride / ethanol / 65 °C / 760.05 Torr / Inert atmosphere

3.1: triethylamine / benzene / 760.05 Torr / Reflux; Inert atmosphere

4.1: methanol / 0.5 h / 760.05 Torr / Inert atmosphere

4.2: 20 °C / 760.05 Torr / Inert atmosphere

5.1: hydrazine / ethanol / 60 °C / 760.05 Torr / Inert atmosphere

With hydrogenchloride; triethylamine; hydrazine; In 1-methyl-pyrrolidin-2-one; methanol; ethanol; benzene;

Reference yield:

: 1533425-10-3
4-amino-2-(trifluoromethylsulfonyl)benzonitrile

: 1533424-22-4
4-(5-amino-1H-[1,2,4]triazol-3-ylamino)-2-trifluoromethanesulfonylbenzonitrile

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / benzene / 760.05 Torr / Reflux; Inert atmosphere

2.1: methanol / 0.5 h / 760.05 Torr / Inert atmosphere

2.2: 20 °C / 760.05 Torr / Inert atmosphere

3.1: hydrazine / ethanol / 60 °C / 760.05 Torr / Inert atmosphere

With triethylamine; hydrazine; In methanol; ethanol; benzene;