3,3,5,5-tetrabenzyl-1,2,4-trithiole

Base Information

• Chemical Name: 3,3,5,5-tetrabenzyl-1,2,4-trithiole
• CAS No.: 103820-69-5
• Molecular Formula: C₃₀H₂₈S₃
• Molecular Weight: 484.75
• Mol file: 103820-69-5.mol

Synonyms:3,3,5,5-tetrabenzyl-1,2,4-trithiole

Chemical Property of 3,3,5,5-tetrabenzyl-1,2,4-trithiole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 3,3,5,5-tetrabenzyl-1,2,4-trithiole

There total 2 articles about 3,3,5,5-tetrabenzyl-1,2,4-trithiole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

1,3-diphenyl-2,2-dimercaptopropane (42937-97-3) → 3,3,5,5-tetrabenzyl-1,2,4-trithiole (103820-69-5)

Guidance literature:

With iodine; In benzene; at 20 ℃; for 48h; Cooling with ice;

DOI:10.1016/j.cclet.2013.05.041

Reference yield:

→ 3,3,5,5-tetrabenzyl-1,2,4-trithiole (103820-69-5)

Guidance literature:

Neben Bis-<1,3-diphenyl-propenyl-(2)>-sulfid aus 1,3-Diphenyl-propan-2,2-dithiol und I2 in Bzl.;

DOI:10.1021/jo01059a089

Reference yield: 90.0%

3,3,5,5-tetrabenzyl-1,2,4-trithiole (103820-69-5) → 1,2-bis(1,3-diphenylpropan-2-yl)disulfane (29671-64-5)

Guidance literature:

With hydrogenchloride; In water; at 0 - 78 ℃; for 1.5h;

DOI:10.1016/j.cclet.2013.05.041

upstream raw materials:

1,3-diphenyl-2,2-dimercaptopropane

Downstream raw materials:

1,2-bis(1,3-diphenylpropan-2-yl)disulfane