1-(2-deoxy-2-methylene-6-O-trityl-β-D-lyxo-hexopyranosyl-2-ulose)thymine

Base Information

• Chemical Name: 1-(2-deoxy-2-methylene-6-O-trityl-β-D-lyxo-hexopyranosyl-2-ulose)thymine
• CAS No.: 946496-68-0
• Molecular Formula: C₃₁H₃₀N₂O₆
• Molecular Weight: 526.589

Synonyms:1-(2-deoxy-2-methylene-6-O-trityl-β-D-lyxo-hexopyranosyl-2-ulose)thymine

Chemical Property of 1-(2-deoxy-2-methylene-6-O-trityl-β-D-lyxo-hexopyranosyl-2-ulose)thymine

Chemical Property:

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Technology Process of 1-(2-deoxy-2-methylene-6-O-trityl-β-D-lyxo-hexopyranosyl-2-ulose)thymine

There total 1 articles about 1-(2-deoxy-2-methylene-6-O-trityl-β-D-lyxo-hexopyranosyl-2-ulose)thymine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

1-(2-deoxy-2-methylene-β-D-lyxo-hexopyranosyl-2-ulose)thymine + trityl chloride (76-83-5) → 1-(2-deoxy-2-methylene-6-O-trityl-β-D-lyxo-hexopyranosyl-2-ulose)thymine (946496-68-0)

Guidance literature:

With pyridine; dmap; at 25 ℃; for 4h;

DOI:10.1016/j.bmc.2007.05.055

Reference yield: 56.0%

1-(2-deoxy-2-methylene-6-O-trityl-β-D-lyxo-hexopyranosyl-2-ulose)thymine (946496-68-0) → 1-(2,3,4-trideoxy-2-methylene-6-O-trityl-β-D-glycero-hex-3-enopyranosyl)thymine

Guidance literature:

With 1H-imidazole; iodine; triphenylphosphine; In N,N-dimethyl-formamide; toluene; for 1h; Heating;

DOI:10.1016/j.bmc.2007.05.055

Reference yield: 21.0%

1-(2-deoxy-2-methylene-6-O-trityl-β-D-lyxo-hexopyranosyl-2-ulose)thymine (946496-68-0) + iodoform (75-47-8) → 1-(2,3,4-trideoxy-2-methylene-6-O-trityl-β-D-glycero-hex-3-enopyranosyl)thymine + C32H29N2O4I3

Guidance literature:

With 1H-imidazole; triphenylphosphine; In N,N-dimethyl-formamide; toluene; for 1h; Heating;

DOI:10.1016/j.bmc.2007.05.055

upstream raw materials:

trityl chloride

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