C₂₉H₄₆O₆Si

Base Information

Chemical Name:C₂₉H₄₆O₆Si
CAS No.:1401427-08-4
Molecular Formula:C₂₉H₄₆O₆Si
Molecular Weight:518.766
Hs Code.:

C<sub>29</sub>H<sub>46</sub>O<sub>6</sub>Si

Synonyms:C₂₉H₄₆O₆Si

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Chemical Property of C₂₉H₄₆O₆Si

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Technology Process of C₂₉H₄₆O₆Si

There total 11 articles about C₂₉H₄₆O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1401427-07-3
C₃₇H₅₆O₆Si₂

: 1401427-08-4
C₂₉H₄₆O₆Si

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at -78 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/ja307207q

Reference yield:

: 1401427-03-9
C₂₈H₄₀O₅Si

: 1401427-08-4
C₂₉H₄₆O₆Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: diethylzinc / toluene; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.5 h / -78 - 0 °C / Inert atmosphere

1.3: 0.33 h / -78 - -20 °C / Inert atmosphere

2.1: cerium(III) chloride; lithium chloride / diethyl ether; tetrahydrofuran / 3 h / -78 °C / Inert atmosphere

2.2: 2.5 h / -78 - 0 °C / Inert atmosphere

3.1: pyridinium p-toluenesulfonate / benzene / 3.17 h / 20 °C / Inert atmosphere

4.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / -78 - -5 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / -78 °C / Inert atmosphere

With cerium(III) chloride; tetrabutyl ammonium fluoride; diethylzinc; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; lithium chloride; In tetrahydrofuran; diethyl ether; dichloromethane; toluene; benzene;
DOI:10.1021/ja307207q

Reference yield:

: C₃₁H₅₀O₅Si₂

: 1401427-08-4
C₂₉H₄₆O₆Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 3 h / 20 °C / Inert atmosphere

2.1: diethylzinc / toluene; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.2: 0.5 h / -78 - 0 °C / Inert atmosphere

2.3: 0.33 h / -78 - -20 °C / Inert atmosphere

3.1: cerium(III) chloride; lithium chloride / diethyl ether; tetrahydrofuran / 3 h / -78 °C / Inert atmosphere

3.2: 2.5 h / -78 - 0 °C / Inert atmosphere

4.1: pyridinium p-toluenesulfonate / benzene / 3.17 h / 20 °C / Inert atmosphere

5.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / -78 - -5 °C / Inert atmosphere

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / -78 °C / Inert atmosphere

With cerium(III) chloride; tetrabutyl ammonium fluoride; diethylzinc; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium chloride; In tetrahydrofuran; diethyl ether; dichloromethane; toluene; benzene;
DOI:10.1021/ja307207q