diethyl 1-(2,2,2-trifluoroethoxy)-1-(4-chloro-3-methoxyphenyl)methanephosphonate

Base Information

Chemical Name:diethyl 1-(2,2,2-trifluoroethoxy)-1-(4-chloro-3-methoxyphenyl)methanephosphonate
CAS No.:220417-58-3
Molecular Formula:C₁₄H₁₉ClF₃O₅P
Molecular Weight:390.724
Hs Code.:

Synonyms:diethyl 1-(2,2,2-trifluoroethoxy)-1-(4-chloro-3-methoxyphenyl)methanephosphonate

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Chemical Property of diethyl 1-(2,2,2-trifluoroethoxy)-1-(4-chloro-3-methoxyphenyl)methanephosphonate

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Technology Process of diethyl 1-(2,2,2-trifluoroethoxy)-1-(4-chloro-3-methoxyphenyl)methanephosphonate

There total 1 articles about diethyl 1-(2,2,2-trifluoroethoxy)-1-(4-chloro-3-methoxyphenyl)methanephosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.6%

: 189942-82-3
4-chloro-3-methoxybenzaldehyde bis-(2,2,2-trifluoroethyl)acetal

: 122-52-1
triethyl phosphite

: 220417-58-3
diethyl 1-(2,2,2-trifluoroethoxy)-1-(4-chloro-3-methoxyphenyl)methanephosphonate

Guidance literature:: 4-chloro-3-methoxybenzaldehyde bis-(2,2,2-trifluoroethyl)acetal; triethyl phosphite; With boron trifluoride diethyl etherate; In dichloromethane; at -8 - 20 ℃; for 43.6667h;

With water; sodium hydrogencarbonate; In dichloromethane; at 20 ℃; for 1h;

Reference yield: 83.1%

: 220417-58-3
diethyl 1-(2,2,2-trifluoroethoxy)-1-(4-chloro-3-methoxyphenyl)methanephosphonate

: 20098-17-3
5-chloroadamantan-2-one

: 189942-78-7
2-chloro-5-{1-(2,2,2-trifluoroethoxy-5'-chloro-tricyclo[3.3.1.1^3,7]dec-2-ylidenemethyl)} anisole

Guidance literature:: diethyl 1-(2,2,2-trifluoroethoxy)-1-(4-chloro-3-methoxyphenyl)methanephosphonate; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.583333h;

5-chloroadamantan-2-one; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 2.55h; Heating / reflux;

With water; sodium hydrogencarbonate; In tetrahydrofuran; hexane; at 20 ℃;