C₂₉H₄₀O₆

Base Information

Chemical Name:C₂₉H₄₀O₆
CAS No.:1209386-09-3
Molecular Formula:C₂₉H₄₀O₆
Molecular Weight:484.633
Hs Code.:

C<sub>29</sub>H<sub>40</sub>O<sub>6</sub>

Synonyms:C₂₉H₄₀O₆

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Chemical Property of C₂₉H₄₀O₆

Chemical Property:

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Technology Process of C₂₉H₄₀O₆

There total 7 articles about C₂₉H₄₀O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1209385-80-7
C₂₉H₃₈O₆

: 1209386-09-3
C₂₉H₄₀O₆

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; formic acid; tributylphosphine; triethylamine; In 1,4-dioxane; at 20 ℃; for 9.5h; Inert atmosphere;
DOI:10.1021/jo400260m

Reference yield:

: C₁₉H₂₈O₄

: 1209386-09-3
C₂₉H₄₀O₆

Guidance literature:: Multi-step reaction with 6 steps

1: trifluorormethanesulfonic acid / dichloromethane; cyclohexane / 0.5 h / 20 °C / Inert atmosphere

2: diisobutylaluminium hydride / dichloromethane; hexane / 0.08 h / -78 °C / Inert atmosphere

3: L-(+)-diisopropyl tartrate; titanium(IV) isopropylate; tert.-butylhydroperoxide / dichloromethane; decane / -20 °C / Inert atmosphere; Molecular sieve

4: dimethyl sulfoxide; sulfur trioxide pyridine complex; triethylamine / dichloromethane / 1.5 h / 0 °C / Inert atmosphere

5: dichloromethane / 0.02 h / 0 °C / Inert atmosphere

6: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; tributylphosphine; formic acid; triethylamine / 1,4-dioxane / 9.5 h / 20 °C / Inert atmosphere

With titanium(IV) isopropylate; tert.-butylhydroperoxide; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; formic acid; L-(+)-diisopropyl tartrate; tributylphosphine; trifluorormethanesulfonic acid; sulfur trioxide pyridine complex; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; In 1,4-dioxane; decane; hexane; dichloromethane; cyclohexane; 3: |Sharpless Asymmetric Epoxidation / 4: |Parikh-Doering Oxidation / 5: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1021/jo400260m

Reference yield:

: C₂₇H₃₆O₅

: 1209386-09-3
C₂₉H₄₀O₆

Guidance literature:: Multi-step reaction with 5 steps

1: diisobutylaluminium hydride / dichloromethane; hexane / 0.08 h / -78 °C / Inert atmosphere

2: L-(+)-diisopropyl tartrate; titanium(IV) isopropylate; tert.-butylhydroperoxide / dichloromethane; decane / -20 °C / Inert atmosphere; Molecular sieve

3: dimethyl sulfoxide; sulfur trioxide pyridine complex; triethylamine / dichloromethane / 1.5 h / 0 °C / Inert atmosphere

4: dichloromethane / 0.02 h / 0 °C / Inert atmosphere

5: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; tributylphosphine; formic acid; triethylamine / 1,4-dioxane / 9.5 h / 20 °C / Inert atmosphere

With titanium(IV) isopropylate; tert.-butylhydroperoxide; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; formic acid; L-(+)-diisopropyl tartrate; tributylphosphine; sulfur trioxide pyridine complex; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; In 1,4-dioxane; decane; hexane; dichloromethane; 2: |Sharpless Asymmetric Epoxidation / 3: |Parikh-Doering Oxidation / 4: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1021/jo400260m