N-ethyl-N-methyl-N'-{4-[3-(1,1,2,2-tetrafluoroethoxy)phenylthio]-2,5-xylyl}formamidine

Base Information

Chemical Name:N-ethyl-N-methyl-N'-{4-[3-(1,1,2,2-tetrafluoroethoxy)phenylthio]-2,5-xylyl}formamidine
CAS No.:1361044-71-4
Molecular Formula:C₂₀H₂₂F₄N₂OS
Molecular Weight:414.467
Hs Code.:

Synonyms:N-ethyl-N-methyl-N'-{4-[3-(1,1,2,2-tetrafluoroethoxy)phenylthio]-2,5-xylyl}formamidine

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Chemical Property of N-ethyl-N-methyl-N'-{4-[3-(1,1,2,2-tetrafluoroethoxy)phenylthio]-2,5-xylyl}formamidine

Chemical Property:

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Technology Process of N-ethyl-N-methyl-N'-{4-[3-(1,1,2,2-tetrafluoroethoxy)phenylthio]-2,5-xylyl}formamidine

There total 5 articles about N-ethyl-N-methyl-N'-{4-[3-(1,1,2,2-tetrafluoroethoxy)phenylthio]-2,5-xylyl}formamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40248-84-8
3-mercaptophenol

: 1361044-71-4
N-ethyl-N-methyl-N'-{4-[3-(1,1,2,2-tetrafluoroethoxy)phenylthio]-2,5-xylyl}formamidine

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

2.1: acetic acid; iron / ethanol; water / 1.5 h / 60 - 90 °C

3.1: toluene-4-sulfonic acid / 3 h / Reflux

3.2: 3 h / 40 °C

4.1: potassium hydroxide / toluene; dimethyl sulfoxide / 1 h / -25 °C

With iron; potassium carbonate; acetic acid; potassium hydroxide; toluene-4-sulfonic acid; In ethanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;

Reference yield:

: 116-14-3,82785-14-6
polytetrafluoroethylene

: 1361046-23-2
N-ethyl-N-methyl-N'-[4-(3-hydroxyphenylthio)-2,5-xylyl]formamidine

: 1361044-71-4
N-ethyl-N-methyl-N'-{4-[3-(1,1,2,2-tetrafluoroethoxy)phenylthio]-2,5-xylyl}formamidine

Guidance literature:: With potassium hydroxide; In dimethyl sulfoxide; toluene; at -25 ℃; for 1h;

Reference yield:

: 1374025-94-1
2-nitro-5-(3-hydroxyphenylthio)-p-xylene

: 1361044-71-4
N-ethyl-N-methyl-N'-{4-[3-(1,1,2,2-tetrafluoroethoxy)phenylthio]-2,5-xylyl}formamidine

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid; iron / ethanol; water / 1.5 h / 60 - 90 °C

2.1: toluene-4-sulfonic acid / 3 h / Reflux

2.2: 3 h / 40 °C

3.1: potassium hydroxide / toluene; dimethyl sulfoxide / 1 h / -25 °C

With iron; acetic acid; potassium hydroxide; toluene-4-sulfonic acid; In ethanol; water; dimethyl sulfoxide; toluene;