4-(6-bromo-5-methyl-thieno[2,3-d]pyrimidin-4-ylamino)-3-ethoxy-benzamide

Base Information

Chemical Name:4-(6-bromo-5-methyl-thieno[2,3-d]pyrimidin-4-ylamino)-3-ethoxy-benzamide
CAS No.:1332721-00-2
Molecular Formula:C₁₆H₁₅BrN₄O₂S
Molecular Weight:407.291
Hs Code.:

Synonyms:4-(6-bromo-5-methyl-thieno[2,3-d]pyrimidin-4-ylamino)-3-ethoxy-benzamide

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Chemical Property of 4-(6-bromo-5-methyl-thieno[2,3-d]pyrimidin-4-ylamino)-3-ethoxy-benzamide

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Technology Process of 4-(6-bromo-5-methyl-thieno[2,3-d]pyrimidin-4-ylamino)-3-ethoxy-benzamide

There total 5 articles about 4-(6-bromo-5-methyl-thieno[2,3-d]pyrimidin-4-ylamino)-3-ethoxy-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 917908-06-6
3-ethoxy-4-(5-methyl-thieno[2,3-d]pyrimidin-4-ylamino)-benzamide

: 1332721-00-2
4-(6-bromo-5-methyl-thieno[2,3-d]pyrimidin-4-ylamino)-3-ethoxy-benzamide

Guidance literature:: With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; for 3h; Reflux;

Reference yield:

: 3556-52-3
3-fluoro-4-nitro-benzamide

: 1332721-00-2
4-(6-bromo-5-methyl-thieno[2,3-d]pyrimidin-4-ylamino)-3-ethoxy-benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydride / tetrahydrofuran / 0.5 h / 20 °C / Cooling with ice

2: ammonium formate / palladium on activated charcoal / methanol / 2 h / Reflux

3: toluene-4-sulfonic acid / isopropyl alcohol / 20 h / 100 °C

4: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / tetrachloromethane / 3 h / Reflux

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); ammonium formate; sodium hydride; toluene-4-sulfonic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; tetrachloromethane; isopropyl alcohol;

Reference yield:

: 917909-46-7
3-ethoxy-4-nitro-benzoic acid amide

: 1332721-00-2
4-(6-bromo-5-methyl-thieno[2,3-d]pyrimidin-4-ylamino)-3-ethoxy-benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium formate / palladium on activated charcoal / methanol / 2 h / Reflux

2: toluene-4-sulfonic acid / isopropyl alcohol / 20 h / 100 °C

3: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / tetrachloromethane / 3 h / Reflux

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); ammonium formate; toluene-4-sulfonic acid; palladium on activated charcoal; In methanol; tetrachloromethane; isopropyl alcohol;