tert-Butyldimethylsilyl 2-azido-4-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-6-O-benzyl-2-deoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranoside

Base Information

Chemical Name:tert-Butyldimethylsilyl 2-azido-4-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-6-O-benzyl-2-deoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranoside
CAS No.:120312-19-8
Molecular Formula:C₄₃H₅₈N₆O₁₁Si
Molecular Weight:863.053
Hs Code.:

tert-Butyldimethylsilyl 2-azido-4-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-6-O-benzyl-2-deoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranoside

Synonyms:tert-Butyldimethylsilyl 2-azido-4-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-6-O-benzyl-2-deoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranoside

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Chemical Property of tert-Butyldimethylsilyl 2-azido-4-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-6-O-benzyl-2-deoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranoside

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Technology Process of tert-Butyldimethylsilyl 2-azido-4-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-6-O-benzyl-2-deoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranoside

There total 18 articles about tert-Butyldimethylsilyl 2-azido-4-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-6-O-benzyl-2-deoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: tert-Butyldimethylsilyl 2-azido-4-O-(2-azido-3,6-di-O-benzyl-2-deoxy-4-O-tetrahydropyranyl-β-D-glucopyranosyl)-6-O-benzyl-2-deoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranoside

: 120312-19-8
tert-Butyldimethylsilyl 2-azido-4-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-6-O-benzyl-2-deoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranoside

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 2h; Ambient temperature;

Reference yield: 29.0%

: 120312-12-1
tert-Butyldimethylsilyl-2-azido-4-O-(4-O-allyl-2-azido-3,6-di-O-benzyl-2-desoxy-β-D-glucopyranosyl)-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranosid

: 120312-19-8
tert-Butyldimethylsilyl-2-azido-4-O-(2-azido-3,6-di-O-benzyl-2-desoxy-β-D-glucopyranosyl)-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranosid

: 120385-02-6
(R)-2-[(2S,3R,4R,5S,6R)-3-Azido-5-((2S,3R,4R,5S,6R)-3-azido-4-benzyloxy-6-benzyloxymethyl-5-propoxy-tetrahydro-pyran-2-yloxy)-6-benzyloxymethyl-2-(tert-butyl-dimethyl-silanyloxy)-tetrahydro-pyran-4-yloxy]-propionic acid methyl ester

Guidance literature:: With water; 1,8-diazabicyclo[5.4.0]undec-7-ene; ; In ethanol; for 7h; Heating;

Reference yield:

: 17674-16-7
benzyl triflate

: 120312-19-8
tert-Butyldimethylsilyl-2-azido-4-O-(2-azido-3,6-di-O-benzyl-2-desoxy-β-D-glucopyranosyl)-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 2,6-di-tert-butylpyridine; 2.) pyridine / 1.) CH₂CL₂, -65 deg C, 20 h; 2.) H₂O, 20 deg C

2: 87 percent / 0.1M BF₃*Et₂O / CH₂Cl₂; hexane / 4 h / -20 °C

3: 1.) H₂O, 1,8-diazabicyclo<5.4.0>undec-7-en; 2.) 60percent CF₃COOH / 1.) 3)>, reflux, 7 h; 2.) CH₂Cl₂, room temp., 1.5 h

With pyridine; 2,6-di-tert-butyl-pyridine; boron trifluoride diethyl etherate; water; 1,8-diazabicyclo[5.4.0]undec-7-ene; trifluoroacetic acid; In hexane; dichloromethane;