N-benzyloxycarbonyl-D-asparagine methyl ester

Base Information

Chemical Name:N-benzyloxycarbonyl-D-asparagine methyl ester
CAS No.:160348-02-7
Molecular Formula:C₁₃H₁₆N₂O₅
Molecular Weight:280.28
Hs Code.:

Synonyms:N-benzyloxycarbonyl-D-asparagine methyl ester

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Chemical Property of N-benzyloxycarbonyl-D-asparagine methyl ester

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Technology Process of N-benzyloxycarbonyl-D-asparagine methyl ester

There total 3 articles about N-benzyloxycarbonyl-D-asparagine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 126401-11-4,4668-38-6
N-benzyloxycarbonyl-D,L-asparagine ethyl ester

: 160348-02-7
N-benzyloxycarbonyl-D-asparagine methyl ester

: 4668-38-6
N-benzyloxycarbonyl-D-asparagine ethyl ester

Guidance literature:: With sodium hydroxide; savinase 16L; sodium chloride; In tetrahydrofuran; phosphate buffer; for 17h; pH=6.5;
DOI:10.1016/j.tet.2003.10.118

Reference yield: 46.0%

: 160348-01-6
N-benzyloxycarbonyl-D,L-asparagine methyl ester

: 2304-96-3
N-benzyloxycarbonyl-L-asparagine

: 160348-02-7
N-benzyloxycarbonyl-D-asparagine methyl ester

Guidance literature:: With sodium hydroxide; Alcalase 2.4L from Bacillus sp; sodium chloride; In tetrahydrofuran; phosphate buffer; for 16h; pH=6.5;
DOI:10.1016/j.tet.2003.10.118

Reference yield:

: 29880-22-6
N-benzyloxy-carbonyl-DL-asparagine

: 160348-02-7
N-benzyloxycarbonyl-D-asparagine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / SOCl₂ / 0.25 h / 0 °C

2: Alcalase 2.4L from Bacillus sp.; NaCl; NaOH / aq. phosphate buffer; tetrahydrofuran / 2.1 h / pH 6.5

With sodium hydroxide; thionyl chloride; Alcalase 2.4L from Bacillus sp; sodium chloride; In tetrahydrofuran; phosphate buffer;
DOI:10.1016/j.tet.2003.10.118