C₂₁H₂₃N₅OS

Base Information

Chemical Name:C₂₁H₂₃N₅OS
CAS No.:1248501-52-1
Molecular Formula:C₂₁H₂₃N₅OS
Molecular Weight:393.513
Hs Code.:

C<sub>21</sub>H<sub>23</sub>N<sub>5</sub>OS

Synonyms:C₂₁H₂₃N₅OS

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Chemical Property of C₂₁H₂₃N₅OS

Chemical Property:

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Technology Process of C₂₁H₂₃N₅OS

There total 8 articles about C₂₁H₂₃N₅OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 1248504-39-3
C₂₆H₃₁N₅O₃S

: 1248501-52-1
C₂₁H₂₃N₅OS

Guidance literature:: C₂₆H₃₁N₅O₃S; With formic acid; at 20 ℃; for 18h;

With sodium hydrogencarbonate; In water;

Reference yield:

: 621-50-1
(3-nitrophenyl)acetonitrile

: 1248501-52-1
C₂₁H₂₃N₅OS

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydride / diethyl ether; dimethyl sulfoxide; mineral oil / 3.58 h / 20 - 35 °C

2.1: borane-THF / tetrahydrofuran / 2.5 h / Reflux

3.1: acetone / 0.5 h / 20 °C

4.1: sodium hydroxide; water / methanol / 0.33 h / 50 °C

5.1: acetonitrile / 3 h / 50 °C

5.2: 2 h / 20 °C

6.1: water; ammonium chloride; iron / tetrahydrofuran; methanol / 2.5 h / Reflux

7.1: triethylamine; chlorophosphoric acid diphenyl ester / ethyl acetate / 0.25 h / 20 °C

8.1: formic acid / 18 h / 20 °C

With formic acid; borane-THF; water; iron; sodium hydride; ammonium chloride; triethylamine; chlorophosphoric acid diphenyl ester; sodium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dimethyl sulfoxide; ethyl acetate; acetone; acetonitrile; mineral oil;

Reference yield:

: 1067192-37-3
1-(3-nitro-phenyl)-cyclopentanecarbonitrile

: 1248501-52-1
C₂₁H₂₃N₅OS

Guidance literature:: Multi-step reaction with 7 steps

1.1: borane-THF / tetrahydrofuran / 2.5 h / Reflux

2.1: acetone / 0.5 h / 20 °C

3.1: sodium hydroxide; water / methanol / 0.33 h / 50 °C

4.1: acetonitrile / 3 h / 50 °C

4.2: 2 h / 20 °C

5.1: water; ammonium chloride; iron / tetrahydrofuran; methanol / 2.5 h / Reflux

6.1: triethylamine; chlorophosphoric acid diphenyl ester / ethyl acetate / 0.25 h / 20 °C

7.1: formic acid / 18 h / 20 °C

With formic acid; borane-THF; water; iron; ammonium chloride; triethylamine; chlorophosphoric acid diphenyl ester; sodium hydroxide; In tetrahydrofuran; methanol; ethyl acetate; acetone; acetonitrile;