(3aR,5S,6R,6aR)-2,2-Dimethyl-6-nitroso-5-trityloxymethyl-tetrahydro-furo[2,3-d][1,3]dioxole

Base Information

Chemical Name:(3aR,5S,6R,6aR)-2,2-Dimethyl-6-nitroso-5-trityloxymethyl-tetrahydro-furo[2,3-d][1,3]dioxole
CAS No.:143416-86-8
Molecular Formula:C₂₇H₂₇NO₅
Molecular Weight:445.515
Hs Code.:

Synonyms:(3aR,5S,6R,6aR)-2,2-Dimethyl-6-nitroso-5-trityloxymethyl-tetrahydro-furo[2,3-d][1,3]dioxole

Suppliers and Price of (3aR,5S,6R,6aR)-2,2-Dimethyl-6-nitroso-5-trityloxymethyl-tetrahydro-furo[2,3-d][1,3]dioxole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3aR,5S,6R,6aR)-2,2-Dimethyl-6-nitroso-5-trityloxymethyl-tetrahydro-furo[2,3-d][1,3]dioxole

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Technology Process of (3aR,5S,6R,6aR)-2,2-Dimethyl-6-nitroso-5-trityloxymethyl-tetrahydro-furo[2,3-d][1,3]dioxole

There total 1 articles about (3aR,5S,6R,6aR)-2,2-Dimethyl-6-nitroso-5-trityloxymethyl-tetrahydro-furo[2,3-d][1,3]dioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 106966-48-7
desoxy-3-hydroxyamino-3-O-isopropylidene-1,2-O-trityl-5-α-D-ribofuranose

: 143416-86-8
(3aR,5S,6R,6aR)-2,2-Dimethyl-6-nitroso-5-trityloxymethyl-tetrahydro-furo[2,3-d][1,3]dioxole

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In chloroform; for 2h; Ambient temperature;

Reference yield: 72.0%

: 143416-86-8
(3aR,5S,6R,6aR)-2,2-Dimethyl-6-nitroso-5-trityloxymethyl-tetrahydro-furo[2,3-d][1,3]dioxole

: 1165952-91-9
cyclohexa-1,3-diene

: 143416-92-6
(1S,4R)-3-((3aR,5S,6R,6aR)-2,2-Dimethyl-5-trityloxymethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl)-2-oxa-3-aza-bicyclo[2.2.2]oct-5-ene

Guidance literature:: In chloroform; for 2h; Heating;

Reference yield:

: 143416-86-8
(3aR,5S,6R,6aR)-2,2-Dimethyl-6-nitroso-5-trityloxymethyl-tetrahydro-furo[2,3-d][1,3]dioxole

: 143417-01-0
(1S,4R)-4-[((3aR,5S,6R,6aR)-2,2-Dimethyl-5-trityloxymethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl)-hydroxy-amino]-cyclohex-2-enol

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / CHCl₃ / 2 h / Heating

2: 39 percent / m-chloroperbenzoic acid / CHCl₃ / 1.5 h / Ambient temperature

3: 76 percent / NaBH₃CN, aq. HCl / methanol

With hydrogenchloride; sodium cyanoborohydride; 3-chloro-benzenecarboperoxoic acid; In methanol; chloroform;