Technology Process of 3-n-propyl sufide
There total 4 articles about 3-n-propyl sufide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
3-(10-deoxoartemisin-10-yl)propanoic acid;
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane;
for 1h;
3-n-propylsulfanylaniline;
In
dichloromethane;
at 20 ℃;
for 8h;
DOI:10.1021/jm201214d
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tin(IV) chloride
2: dimethylsulfide borane complex; sodium peroxoborate tetrahydrate
3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / benzotriazol-1-ol / dichloromethane / 8 h / 20 °C
With
sodium peroxoborate tetrahydrate; dimethylsulfide borane complex; tin(IV) chloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
benzotriazol-1-ol;
In
dichloromethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium perborate tetrahydrate; dimethyl sulfide borane
2.1: sodium periodate; ruthenium trichloride
3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h
3.2: 8 h / 20 °C
With
ruthenium trichloride; sodium periodate; sodium perborate tetrahydrate; dimethyl sulfide borane; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane;
DOI:10.1021/jm201214d
