Technology Process of C46H43BF2N10O11
There total 9 articles about C46H43BF2N10O11 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
((O2N)2C6H3CH2OC6H3(COOH)C(C4N(CH3)2CH2CH2COOH)2)BF2;
With
1-hydroxy-pyrrolidine-2,5-dione; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dimethyl sulfoxide;
at 20 ℃;
for 2h;
6-[[4-(aminomethyl)phenyl]methoxy]-7H-purin-2-amine;
With
triethylamine;
In
dimethyl sulfoxide;
DOI:10.1021/ja212125w
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / methanol / 20 °C
2: potassium tert-butylate / N,N-dimethyl-formamide / 20 °C
3: potassium carbonate / methanol; water / Reflux
4: 1-hydroxy-pyrrolidine-2,5-dione; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dimethyl sulfoxide / 2 h / 20 °C
With
1-hydroxy-pyrrolidine-2,5-dione; potassium tert-butylate; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
methanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ja212125w
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / acetone / 80 °C
2: sodium hydroxide / water; acetone / 1.5 h / 50 °C
3: 1-hydroxy-pyrrolidine-2,5-dione; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dimethyl sulfoxide / 2 h / 20 °C
With
1-hydroxy-pyrrolidine-2,5-dione; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide;
In
water; dimethyl sulfoxide; acetone;
DOI:10.1021/ja212125w
