C₅₆H₉₆O₁₀Si₂

Base Information

Chemical Name:C₅₆H₉₆O₁₀Si₂
CAS No.:930803-60-4
Molecular Formula:C₅₆H₉₆O₁₀Si₂
Molecular Weight:985.543
Hs Code.:

C<sub>56</sub>H<sub>96</sub>O<sub>10</sub>Si<sub>2</sub>

Synonyms:C₅₆H₉₆O₁₀Si₂

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Chemical Property of C₅₆H₉₆O₁₀Si₂

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Technology Process of C₅₆H₉₆O₁₀Si₂

There total 20 articles about C₅₆H₉₆O₁₀Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 930803-40-0
C₅₉H₁₀₂O₉S₂Si₂

: 930803-60-4
C₅₆H₉₆O₁₀Si₂

Guidance literature:: With bis-[(trifluoroacetoxy)iodo]benzene; In tetrahydrofuran; methanol; water; at 20 ℃;
DOI:10.1002/anie.200604053

Reference yield:

: 930803-25-1
C₁₀H₁₅S₂O₂Br

: 930803-60-4
C₅₆H₉₆O₁₀Si₂

Guidance literature:: Multi-step reaction with 8 steps

1: 99 percent / diisobutylaluminum hydride / CH₂Cl₂ / -45 °C

2: 70 percent / methanesulfonyl chloride; triethylamine; 4-(dimethylamino)pyridine / lithium bromide / CH₂Cl₂; dimethylformamide

3: 99 percent / LiBHEt₃ / tetrahydrofuran / 0 °C

4: 80 percent / tert-butyllithium / tetrahydrofuran / -96 - -78 °C

5: 83 percent / Zn(BH₄)2 / diethyl ether / 2 h / -20 °C

6: 93 percent / imidazole / dimethylformamide / 50 °C

7: 81 percent / tert-butyllithium; hexamethylphosphoramide / tetrahydrofuran / -78 - -40 °C

8: 83 percent / (bis(trifluoroacetoxy)iodo)benzene / tetrahydrofuran; H₂O; methanol / 20 °C

With 1H-imidazole; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; zinc(II) tetrahydroborate; tert.-butyl lithium; diisobutylaluminium hydride; lithium triethylborohydride; methanesulfonyl chloride; triethylamine; bis-[(trifluoroacetoxy)iodo]benzene; lithium bromide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/anie.200604053

Reference yield:

: 930803-26-2
C₉H₁₅S₂OBr

: 930803-60-4
C₅₆H₉₆O₁₀Si₂

Guidance literature:: Multi-step reaction with 7 steps

1: 70 percent / methanesulfonyl chloride; triethylamine; 4-(dimethylamino)pyridine / lithium bromide / CH₂Cl₂; dimethylformamide

2: 99 percent / LiBHEt₃ / tetrahydrofuran / 0 °C

3: 80 percent / tert-butyllithium / tetrahydrofuran / -96 - -78 °C

4: 83 percent / Zn(BH₄)2 / diethyl ether / 2 h / -20 °C

5: 93 percent / imidazole / dimethylformamide / 50 °C

6: 81 percent / tert-butyllithium; hexamethylphosphoramide / tetrahydrofuran / -78 - -40 °C

7: 83 percent / (bis(trifluoroacetoxy)iodo)benzene / tetrahydrofuran; H₂O; methanol / 20 °C

With 1H-imidazole; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; zinc(II) tetrahydroborate; tert.-butyl lithium; lithium triethylborohydride; methanesulfonyl chloride; triethylamine; bis-[(trifluoroacetoxy)iodo]benzene; lithium bromide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/anie.200604053