12,12-Dimethyl-1,7-diphenyl-8,11-diazahexacyclo<5.4.1.0^2,6.0^3,10.0^5,9.0^8,11>dodecan

Base Information

• Chemical Name: 12,12-Dimethyl-1,7-diphenyl-8,11-diazahexacyclo<5.4.1.0^2,6.0^3,10.0^5,9.0^8,11>dodecan
• CAS No.: 105834-60-4
• Molecular Formula: C₂₄H₂₄N₂
• Molecular Weight: 340.468

Synonyms:12,12-Dimethyl-1,7-diphenyl-8,11-diazahexacyclo<5.4.1.0^2,6.0^3,10.0^5,9.0^8,11>dodecan

Chemical Property of 12,12-Dimethyl-1,7-diphenyl-8,11-diazahexacyclo<5.4.1.0^2,6.0^3,10.0^5,9.0^8,11>dodecan

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Technology Process of 12,12-Dimethyl-1,7-diphenyl-8,11-diazahexacyclo<5.4.1.0^2,6.0^3,10.0^5,9.0^8,11>dodecan

There total 3 articles about 12,12-Dimethyl-1,7-diphenyl-8,11-diazahexacyclo<5.4.1.0^2,6.0^3,10.0^5,9.0^8,11>dodecan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

(1α,4α,4aα,5α,8α,8aα)-1,4,4a,5,8,8a-Hexahydro-9,9-dimethyl-1,4-diphenyl-1,4;5,8-dimethanophthalazin (105879-79-6) → 12,12-Dimethyl-1,7-diphenyl-8,11-diazahexacyclo<5.4.1.02,6.03,10.05,9.08,11>dodecan (105834-60-4)

Guidance literature:

In [D₃]acetonitrile; at -20 ℃; for 0.5h; Irradiation;

Reference yield:

2,2-dimethyl-1,3-diphenylpropane-1,3-dione (41169-42-0) → 12,12-Dimethyl-1,7-diphenyl-8,11-diazahexacyclo<5.4.1.02,6.03,10.05,9.08,11>dodecan (105834-60-4)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂NNH₂*H₂O / CH₂Cl₂ / 3 h / Heating

2: 2 percent / CF₃-COOH / CHCl₃ / 96 h / Heating

3: 86 percent / CD₃CN / 0.5 h / -20 °C / Irradiation

With hydrazine hydrate; trifluoroacetic acid; In dichloromethane; chloroform; [D₃]acetonitrile;

Reference yield:

4,4-dimethyl-3,5-diphenyl-4H-pyrazole (30169-45-0) → 12,12-Dimethyl-1,7-diphenyl-8,11-diazahexacyclo<5.4.1.02,6.03,10.05,9.08,11>dodecan (105834-60-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 2 percent / CF₃-COOH / CHCl₃ / 96 h / Heating

2: 86 percent / CD₃CN / 0.5 h / -20 °C / Irradiation

With trifluoroacetic acid; In chloroform; [D₃]acetonitrile;

upstream raw materials:

(1α,4α,4aα,5α,8α,8aα)-1,4,4a,5,8,8a-Hexahydro-9,9-dimethyl-1,4-diphenyl-1,4;5,8-dimethanophthalazin

2,2-dimethyl-1,3-diphenylpropane-1,3-dione

4,4-dimethyl-3,5-diphenyl-4H-pyrazole

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