(2S,3R)-N-1,2-cyclohexanedicarboxy-4-phenylvaline methyl ester

Base Information

Chemical Name:(2S,3R)-N-1,2-cyclohexanedicarboxy-4-phenylvaline methyl ester
CAS No.:410086-95-2
Molecular Formula:C₂₀H₂₅NO₄
Molecular Weight:343.423
Hs Code.:

Synonyms:(2S,3R)-N-1,2-cyclohexanedicarboxy-4-phenylvaline methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R)-N-1,2-cyclohexanedicarboxy-4-phenylvaline methyl ester

Chemical Property:

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Technology Process of (2S,3R)-N-1,2-cyclohexanedicarboxy-4-phenylvaline methyl ester

There total 2 articles about (2S,3R)-N-1,2-cyclohexanedicarboxy-4-phenylvaline methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: (2S)-N-phthaloyl-4-phenyl-3,4-dehydrovaline methyl ester

: (2S)-N-phthaloyl-4-phenylvaline methyl ester

: 410086-95-2
(2S,3R)-N-1,2-cyclohexanedicarboxy-4-phenylvaline methyl ester

: 410087-16-0
(2S,3S)-N-1,2-cyclohexanedicarboxy-4-phenylvaline methyl ester

Guidance literature:: With platinum(IV) oxide; hydrogen; In ethanol;
DOI:10.1021/jo010176z

Reference yield:

: 137649-44-6
(2S)-N-phthaloyl-3,4-dehydrovaline methyl ester

: 410086-95-2
(2S,3R)-N-1,2-cyclohexanedicarboxy-4-phenylvaline methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / palladium acetate; silver nitrate / acetonitrile / 6 h / 50 °C

2: H₂; PtO₂ / ethanol

With platinum(IV) oxide; hydrogen; palladium diacetate; silver nitrate; In ethanol; acetonitrile; 1: Heck reaction;
DOI:10.1021/jo010176z