2-amino-4,5-dimethylformanilide

Base Information

Chemical Name:2-amino-4,5-dimethylformanilide
CAS No.:132382-43-5
Molecular Formula:C₉H₁₂N₂O
Molecular Weight:164.207
Hs Code.:

Synonyms:2-amino-4,5-dimethylformanilide

Suppliers and Price of 2-amino-4,5-dimethylformanilide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-amino-4,5-dimethylformanilide

Chemical Property:

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Technology Process of 2-amino-4,5-dimethylformanilide

There total 6 articles about 2-amino-4,5-dimethylformanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 171182-96-0
4,5-dimethyl-2-nitroformanilide

: 132382-43-5
2-amino-4,5-dimethylformanilide

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 10h; Time; Temperature; Reagent/catalyst; Solvent;

Reference yield:

: 95-64-7
4-amino-o-xylene

: 132382-43-5
2-amino-4,5-dimethylformanilide

Guidance literature:: Multi-step reaction with 5 steps

1: acetic acid; H₂O / 1 h / 60 °C

2: 70 percent aq. HNO₃, AcOH / 1 h / below 15 deg C

3: KOH, water / methanol / 1 h / 60 °C

4: 91 percent / Ac₂O / 0.5 h / 60 °C

5: 91 percent / H₂ / 5percent Pd/C / 2-methoxy-ethanol / 3 h / 70 °C / 7600 Torr

With potassium hydroxide; water; hydrogen; nitric acid; acetic anhydride; acetic acid; palladium on activated charcoal; In methanol; 2-methoxy-ethanol; water; acetic acid;
DOI:10.1055/s-1995-4088

Reference yield:

: 6970-77-0
N-(4,5-dimethyl-2-nitrophenyl)acetamide

: 132382-43-5
2-amino-4,5-dimethylformanilide

Guidance literature:: Multi-step reaction with 3 steps

1: KOH, water / methanol / 1 h / 60 °C

2: 91 percent / Ac₂O / 0.5 h / 60 °C

3: 91 percent / H₂ / 5percent Pd/C / 2-methoxy-ethanol / 3 h / 70 °C / 7600 Torr

With potassium hydroxide; water; hydrogen; acetic anhydride; palladium on activated charcoal; In methanol; 2-methoxy-ethanol;
DOI:10.1055/s-1995-4088