Technology Process of C26H28FN3O4S
There total 10 articles about C26H28FN3O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
caesium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
acetonitrile;
at 110 ℃;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: sodium hydroxide; dihydrogen peroxide / methanol / 3.33 h / 15 - 20 °C
2: toluene-4-sulfonic acid hydrazide / ethanol / 2.33 h / 20 - 55 °C
3: sodium hydroxide; bromine / 1,4-dioxane; water / 2 h / 0 °C
4: caesium carbonate / N,N-dimethyl-formamide / 0 - 20 °C
5: diethylamine / copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 0 - 20 °C
6: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C
7: caesium carbonate / tetrakis(triphenylphosphine) palladium(0) / acetonitrile / 110 °C
With
dihydrogen peroxide; bromine; caesium carbonate; diethylamine; N-ethyl-N,N-diisopropylamine; toluene-4-sulfonic acid hydrazide; sodium hydroxide;
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0);
In
1,4-dioxane; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine / dimethyl sulfoxide / 20 °C
2: sodium hydroxide; water; dihydrogen peroxide / dimethyl sulfoxide; methanol / 1 h / 20 °C
3: caesium carbonate / tetrakis(triphenylphosphine) palladium(0) / acetonitrile / 110 °C
With
water; dihydrogen peroxide; caesium carbonate; triethylamine; sodium hydroxide;
tetrakis(triphenylphosphine) palladium(0);
In
methanol; dimethyl sulfoxide; acetonitrile;