C₅₅H₅₇O₁₇P₃

Base Information

Chemical Name:C₅₅H₅₇O₁₇P₃
CAS No.:912567-63-6
Molecular Formula:C₅₅H₅₇O₁₇P₃
Molecular Weight:1082.97
Hs Code.:

C<sub>55</sub>H<sub>57</sub>O<sub>17</sub>P<sub>3</sub>

Synonyms:C₅₅H₅₇O₁₇P₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₅H₅₇O₁₇P₃

Chemical Property:

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Technology Process of C₅₅H₅₇O₁₇P₃

There total 11 articles about C₅₅H₅₇O₁₇P₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 912567-62-5
2-benzyl-4-tetrahydrofuran-3-yl 2,6-di-O-benzyl-α-D-glucopyranoside

: 82372-35-8
N,N-diethyl-1,5-dihydro-3H-2,4,3-benzodioxaphosphepin-3-amine

: 912567-63-6
C₅₅H₅₇O₁₇P₃

Guidance literature:: 2-benzyl-4-tetrahydrofuran-3-yl 2,6-di-O-benzyl-α-D-glucopyranoside; N,N-diethyl-1,5-dihydro-3H-2,4,3-benzodioxaphosphepin-3-amine; With imidazole trifluoromethanesulfonate; In dichloromethane; at -40 - 20 ℃;

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -40 ℃;
DOI:10.1021/jm060310d

Reference yield:

: 518332-41-7
2,6-di-O-benzyl-3,4-O-[(2S,3S)-2,3-dimethoxybutan-2,3-yl]-1-phenylsulfinyl-β-D-glucopyranoside

: 912567-63-6
C₅₅H₅₇O₁₇P₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: 78 percent / 2,6-di-tert-butyl-4-methylpyridine / diethyl ether / 8 h / -78 °C

2.1: 82 percent / TBAF / tetrahydrofuran / 20 °C

3.1: tetrahydrofuran / 20 °C

4.1: PhOCSCl; DMAP / acetonitrile / 20 °C

4.2: 93 percent / Bu₃SnH; AIBN / toluene / Heating

5.1: aq. TFA / 20 °C

6.1: Et₃N; DMAP / acetonitrile / 20 °C

7.1: 60 percent / Et₃SiH; TMSOTf / CH₂Cl₂ / 0.33 h / 0 °C

8.1: 86 percent / NaOMe / methanol / 20 °C

9.1: imidazolium triflate / CH₂Cl₂ / -40 - 20 °C

9.2: 85 percent / m-CPBA / CH₂Cl₂ / -40 °C

With triethylsilane; dmap; 2,6-di-tert-butyl-4-methylpyridine; trimethylsilyl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; sodium methylate; imidazole trifluoromethanesulfonate; triethylamine; trifluoroacetic acid; phenylcarbonochloridothioate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; acetonitrile; 3.1: Moffatt oxidation / 5.2: Barton deoxygenation;
DOI:10.1021/jm060310d

Reference yield:

: 196868-07-2
1,2-O-isopropylidene-5-O-(tert-butyl)dimethylsilyl-α-D-ribofuranoside

: 912567-63-6
C₅₅H₅₇O₁₇P₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: 78 percent / 2,6-di-tert-butyl-4-methylpyridine / diethyl ether / 8 h / -78 °C

2.1: 82 percent / TBAF / tetrahydrofuran / 20 °C

3.1: tetrahydrofuran / 20 °C

4.1: PhOCSCl; DMAP / acetonitrile / 20 °C

4.2: 93 percent / Bu₃SnH; AIBN / toluene / Heating

5.1: aq. TFA / 20 °C

6.1: Et₃N; DMAP / acetonitrile / 20 °C

7.1: 60 percent / Et₃SiH; TMSOTf / CH₂Cl₂ / 0.33 h / 0 °C

8.1: 86 percent / NaOMe / methanol / 20 °C

9.1: imidazolium triflate / CH₂Cl₂ / -40 - 20 °C

9.2: 85 percent / m-CPBA / CH₂Cl₂ / -40 °C

With triethylsilane; dmap; 2,6-di-tert-butyl-4-methylpyridine; trimethylsilyl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; sodium methylate; imidazole trifluoromethanesulfonate; triethylamine; trifluoroacetic acid; phenylcarbonochloridothioate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; acetonitrile; 3.1: Moffatt oxidation / 5.2: Barton deoxygenation;
DOI:10.1021/jm060310d