phenyl 2-O-(4-methylbenzyl)-3,4-O-isopropylidene-1-thio-β-L-fucopyranoside

Base Information

Chemical Name:phenyl 2-O-(4-methylbenzyl)-3,4-O-isopropylidene-1-thio-β-L-fucopyranoside
CAS No.:1250436-25-9
Molecular Formula:C₂₃H₂₈O₄S
Molecular Weight:400.539
Hs Code.:

Synonyms:phenyl 2-O-(4-methylbenzyl)-3,4-O-isopropylidene-1-thio-β-L-fucopyranoside

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Chemical Property of phenyl 2-O-(4-methylbenzyl)-3,4-O-isopropylidene-1-thio-β-L-fucopyranoside

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Technology Process of phenyl 2-O-(4-methylbenzyl)-3,4-O-isopropylidene-1-thio-β-L-fucopyranoside

There total 6 articles about phenyl 2-O-(4-methylbenzyl)-3,4-O-isopropylidene-1-thio-β-L-fucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104-82-5
4-Methylbenzyl chloride

: 196397-59-8
phenyl 3,4-O-isopropylidene-1-thio-β-L-fucopyranoside

: 1250436-25-9
phenyl 2-O-(4-methylbenzyl)-3,4-O-isopropylidene-1-thio-β-L-fucopyranoside

Guidance literature:: With tetra-(n-butyl)ammonium hydrogensulfate; sodium hydroxide; at 90 ℃; for 3h;

Reference yield:

: 167612-34-2
phenyl 6-deoxy-2,3,4-tri-O-acetyl-1-thio-β-L-galactopyranoside

: 1250436-25-9
phenyl 2-O-(4-methylbenzyl)-3,4-O-isopropylidene-1-thio-β-L-fucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium methylate; methanol / 2.5 h / 40 °C

1.2: 0.08 h / pH 7

2.1: toluene-4-sulfonic acid / 2,2-dimethoxy-propane / 12 h / 20 °C

3.1: tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide / 3 h / 90 °C

With methanol; sodium methylate; tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide; toluene-4-sulfonic acid; In 2,2-dimethoxy-propane;

Reference yield:

: 108-98-5
thiophenol

: 1250436-25-9
phenyl 2-O-(4-methylbenzyl)-3,4-O-isopropylidene-1-thio-β-L-fucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: boron trifluoride diethyl etherate / toluene / 18 h / 0 - 20 °C

2.1: sodium methylate; methanol / 2.5 h / 40 °C

2.2: 0.08 h / pH 7

3.1: toluene-4-sulfonic acid / 2,2-dimethoxy-propane / 12 h / 20 °C

4.1: tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide / 3 h / 90 °C

With methanol; boron trifluoride diethyl etherate; sodium methylate; tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide; toluene-4-sulfonic acid; In 2,2-dimethoxy-propane; toluene;