(S)-3-((tert-butoxycarbonyl)(isopropyl)amino)-2-(4-chlorophenyl)propionic acid

Base Information

• Chemical Name: (S)-3-((tert-butoxycarbonyl)(isopropyl)amino)-2-(4-chlorophenyl)propionic acid
• CAS No.: 1001179-33-4
• Molecular Formula: C₁₇H₂₄ClNO₄
• Molecular Weight: 341.835

Synonyms:(S)-3-((tert-butoxycarbonyl)(isopropyl)amino)-2-(4-chlorophenyl)propionic acid

Chemical Property of (S)-3-((tert-butoxycarbonyl)(isopropyl)amino)-2-(4-chlorophenyl)propionic acid

Chemical Property:

• Boiling Point: 453.2±40.0 °C(Predicted)
• Density: 1.181±0.06 g/cm3(Predicted)

Purity/Quality:

99%, ^*data from raw suppliers

(2S)-2-(4-chlorophenyl)-3-[(2-methylpropan-2-yl)oxycarbonyl-propan-2-ylamino]propanoicacid 95%+ ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (S)-3-((tert-butoxycarbonyl)(isopropyl)amino)-2-(4-chlorophenyl)propionic acid

There total 28 articles about (S)-3-((tert-butoxycarbonyl)(isopropyl)amino)-2-(4-chlorophenyl)propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

tert-butyl (S)-3-((S)-4-benzyl-2-oxooxazolidin-3-yl)-2-(4-chlorophenyl)-3-oxopropyl(isopropyl)carbamate (1001179-31-2) → (S)-3-((tert-butoxycarbonyl)(isopropyl)amino)-2-(4-chlorophenyl)propionic acid (1001179-33-4)

Guidance literature:

With lithium hydroxide monohydrate; dihydrogen peroxide; In tetrahydrofuran; water; at 0 - 20 ℃;

Reference yield: 100.0%

(E)-3-((tert-butoxycarbonyl)(isopropyl)amino)-2-(4-chlorophenyl)acrylic acid (1489004-27-4) → (S)-3-((tert-butoxycarbonyl)(isopropyl)amino)-2-(4-chlorophenyl)propionic acid (1001179-33-4)

Guidance literature:

With ditrifluoroacetato[(S)-(?)-2,2′-bis(diphenylphosphino)-1,1′-binaphthyl]ruthenium(II); hydrogen; In ethanol; at 60 ℃; for 14h; under 15001.5 Torr; Temperature; Reagent/catalyst; Solvent; Concentration; Pressure; Glovebox; Autoclave; Sealed tube;

Reference yield: 100.0%

(E)-3-((tert-butoxycarbonyl)(isopropyl)amino)-2-(4-chlorophenyl)acrylic acid (1489004-27-4) → (S)-3-((tert-butoxycarbonyl)(isopropyl)amino)-2-(4-chlorophenyl)propionic acid (1001179-33-4) + (R)-3-(tert-butoxycarbonylisopropylamino)-2-(4-chlorophenyl)propionic acid

Guidance literature:

With ditrifluoroacetato[(S)-(?)-2,2′-bis(diphenylphosphino)-1,1′-binaphthyl]ruthenium(II); hydrogen; In ethanol; at 60 ℃; for 14h; under 15001.5 Torr; Reagent/catalyst; Glovebox; Autoclave; Sealed tube;

upstream raw materials:

tert-butyl (S)-3-((S)-4-benzyl-2-oxooxazolidin-3-yl)-2-(4-chlorophenyl)-3-oxopropyl(isopropyl)carbamate

(4-chloro-phenyl)-acetic acid methyl ester

methyl 2-(4-chlorophenyl)acrylate

methyl 2-(4-chlorophenyl)-3-hydroxypropanoate

Downstream raw materials:

(S)-tert-butyl 2-(4-chlorophenyl)-3-(4-(3-methyl-5-phenyl-1H-pyrrolo[2,3-b]pyridin-4-yl)piperazin-1-yl)-3-oxopropyl(isopropyl)carbamate

(S)-tert-butyl 2-(4-chlorophenyl)-3-(4-(5-(5-methyl-1,3,4-oxadiazol-2-yl)-1H-pyrrolo[2,3-b]pyridin-4-yl)piperazin-1-yl)-3-oxopropyl(isopropyl)carbamate

(S)-tert-butyl 3-(4-(3-butyramido-1H-pyrrolo[2,3-b]pyridin-4-yl)piperazin-1-yl)-2-(4-chlorophenyl)-3-oxopropyl(isopropyl)carbamate

(S)-tert-butyl 2-(4-chlorophenyl)-3-(4-(5-(4-fluorophenyl)-1H-pyrrolo[2,3-b]pyridin-4-yl)piperazin-1-yl)-3-oxopropyl(isopropyl)carbamate

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