9-oxo-9-(N'-phenoxyacetyl-hydrazino)-nonanoic acid N'-phenoxyacetyl-hydrazide

Base Information

• Chemical Name: 9-oxo-9-(N'-phenoxyacetyl-hydrazino)-nonanoic acid N'-phenoxyacetyl-hydrazide
• CAS No.: 316144-71-5
• Molecular Formula: C₂₅H₃₂N₄O₆
• Molecular Weight: 484.552
• Mol file: 316144-71-5.mol

Synonyms:9-oxo-9-(N'-phenoxyacetyl-hydrazino)-nonanoic acid N'-phenoxyacetyl-hydrazide

Chemical Property of 9-oxo-9-(N'-phenoxyacetyl-hydrazino)-nonanoic acid N'-phenoxyacetyl-hydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 9-oxo-9-(N'-phenoxyacetyl-hydrazino)-nonanoic acid N'-phenoxyacetyl-hydrazide

There total 1 articles about 9-oxo-9-(N'-phenoxyacetyl-hydrazino)-nonanoic acid N'-phenoxyacetyl-hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

azelainic acid dihydrazide (4080-95-9) + 2-phenoxyacetic acid (122-59-8) → 9-oxo-9-(N'-phenoxyacetyl-hydrazino)-nonanoic acid N'-phenoxyacetyl-hydrazide (316144-71-5)

Guidance literature:

With trichlorophosphate; In acetonitrile; Heating;

DOI:10.1021/jm050021+

Reference yield: 63.0%

9-oxo-9-(N'-phenoxyacetyl-hydrazino)-nonanoic acid N'-phenoxyacetyl-hydrazide (316144-71-5) → C25H28N4O4 (858538-40-6)

Guidance literature:

With trichlorophosphate; In acetonitrile; for 7h; Heating;

DOI:10.1021/jm050021+

Reference yield:

9-oxo-9-(N'-phenoxyacetyl-hydrazino)-nonanoic acid N'-phenoxyacetyl-hydrazide (316144-71-5) → C39H42N6O2

Guidance literature:

Multi-step reaction with 2 steps

1: 63 percent / POCl₃ / acetonitrile / 7 h / Heating

2: 51 percent / 30 h / 150 °C

With trichlorophosphate; In acetonitrile;

DOI:10.1021/jm050021+

upstream raw materials:

azelainic acid dihydrazide

2-phenoxyacetic acid

Downstream raw materials:

C₂₅H₂₈N₄O₄