(2R,3S,4R,5S)-2-(N⁽⁶⁾-benzoyl-adenin-9-yl)-1-(tertbutoxycarbonyl)piperidine-3,4,5-triyl triacetate

Base Information

• Chemical Name: (2R,3S,4R,5S)-2-(N⁽⁶⁾-benzoyl-adenin-9-yl)-1-(tertbutoxycarbonyl)piperidine-3,4,5-triyl triacetate
• CAS No.: 1269050-19-2
• Molecular Formula: C₂₈H₃₂N₆O₉
• Molecular Weight: 596.597

Synonyms:(2R,3S,4R,5S)-2-(N⁽⁶⁾-benzoyl-adenin-9-yl)-1-(tertbutoxycarbonyl)piperidine-3,4,5-triyl triacetate

Chemical Property of (2R,3S,4R,5S)-2-(N⁽⁶⁾-benzoyl-adenin-9-yl)-1-(tertbutoxycarbonyl)piperidine-3,4,5-triyl triacetate

Chemical Property:

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Technology Process of (2R,3S,4R,5S)-2-(N⁽⁶⁾-benzoyl-adenin-9-yl)-1-(tertbutoxycarbonyl)piperidine-3,4,5-triyl triacetate

There total 1 articles about (2R,3S,4R,5S)-2-(N⁽⁶⁾-benzoyl-adenin-9-yl)-1-(tertbutoxycarbonyl)piperidine-3,4,5-triyl triacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

N6-benzoyladenine (4005-49-6) + (2R,3R,4R,5S)-1-(tert-butoxycarbonyl)piperidine-2,3,4,5-tetrayl tetraacetate (1269049-99-1) → (2R,3S,4R,5S)-2-(N(6)-benzoyl-adenin-9-yl)-1-(tertbutoxycarbonyl)piperidine-3,4,5-triyl triacetate (1269050-19-2) + (2S,3S,4R,5S)-2-(N(6)-benzoyl-adenin-9-yl)-1-(tertbutoxycarbonyl)piperidine-3,4,5-triyl triacetate (1269050-21-6)

Guidance literature:

N₆-benzoyladenine; With N,O-bis-(trimethylsilyl)-acetamide; In acetonitrile; for 0.333333h; Inert atmosphere; Reflux;

(2R,3R,4R,5S)-1-(tert-butoxycarbonyl)piperidine-2,3,4,5-tetrayl tetraacetate; With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 0 - 20 ℃; for 2.5h; Inert atmosphere;

With sodium hydrogencarbonate; In water; acetonitrile; Inert atmosphere; Cooling;

DOI:10.1016/j.bmc.2010.11.063

upstream raw materials:

N₆-benzoyladenine

(2R,3R,4R,5S)-1-(tert-butoxycarbonyl)piperidine-2,3,4,5-tetrayl tetraacetate

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