tert-butyl (2-(2,2,2-trifluoroacetamido)ethyl)(2-(tritylamino)ethyl)carbamate

Base Information

Chemical Name:tert-butyl (2-(2,2,2-trifluoroacetamido)ethyl)(2-(tritylamino)ethyl)carbamate
CAS No.:1373763-30-4
Molecular Formula:C₃₀H₃₄F₃N₃O₃
Molecular Weight:541.613
Hs Code.:

Synonyms:tert-butyl (2-(2,2,2-trifluoroacetamido)ethyl)(2-(tritylamino)ethyl)carbamate

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Chemical Property of tert-butyl (2-(2,2,2-trifluoroacetamido)ethyl)(2-(tritylamino)ethyl)carbamate

Chemical Property:

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Technology Process of tert-butyl (2-(2,2,2-trifluoroacetamido)ethyl)(2-(tritylamino)ethyl)carbamate

There total 3 articles about tert-butyl (2-(2,2,2-trifluoroacetamido)ethyl)(2-(tritylamino)ethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1373763-28-0
2,2,2-trifluoro-N-(2-((2-(tritylamino)ethyl)amino)ethyl)-acetamide

: 1373763-30-4
tert-butyl (2-(2,2,2-trifluoroacetamido)ethyl)(2-(tritylamino)ethyl)carbamate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 18h; Inert atmosphere;
DOI:10.1021/jo202561k

Reference yield:

: N-(2-(triphenylmethyl)amino)ethyl-1,2-ethanediamine

: 1373763-30-4
tert-butyl (2-(2,2,2-trifluoroacetamido)ethyl)(2-(tritylamino)ethyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 0 °C / Inert atmosphere

2: triethylamine / dichloromethane / 18 h / 0 - 20 °C / Inert atmosphere

With triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo202561k

Reference yield:

: 76-83-5
trityl chloride

: 1373763-30-4
tert-butyl (2-(2,2,2-trifluoroacetamido)ethyl)(2-(tritylamino)ethyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 5 h / 0 - 20 °C

2: tetrahydrofuran / 0 °C / Inert atmosphere

3: triethylamine / dichloromethane / 18 h / 0 - 20 °C / Inert atmosphere

With triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo202561k