2-{[(E)-2-(5-Methyl-1H-imidazol-4-ylmethylsulfanyl)-ethylimino]-methyl}-phenol

Base Information

• Chemical Name: 2-{[(E)-2-(5-Methyl-1H-imidazol-4-ylmethylsulfanyl)-ethylimino]-methyl}-phenol
• CAS No.: 130106-85-3
• Molecular Formula: C₁₄H₁₇N₃OS
• Molecular Weight: 275.374

Synonyms:2-{[(E)-2-(5-Methyl-1H-imidazol-4-ylmethylsulfanyl)-ethylimino]-methyl}-phenol

Chemical Property of 2-{[(E)-2-(5-Methyl-1H-imidazol-4-ylmethylsulfanyl)-ethylimino]-methyl}-phenol

Chemical Property:

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Technology Process of 2-{[(E)-2-(5-Methyl-1H-imidazol-4-ylmethylsulfanyl)-ethylimino]-methyl}-phenol

There total 2 articles about 2-{[(E)-2-(5-Methyl-1H-imidazol-4-ylmethylsulfanyl)-ethylimino]-methyl}-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

salicylaldehyde (90-02-8) + 2-[((5-methyl-1H-imidazol-4-yl)methyl)thio]ethanamine dihydrochloride (38603-72-4,65197-95-7,72500-47-1) → 2-{[(E)-2-(5-Methyl-1H-imidazol-4-ylmethylsulfanyl)-ethylimino]-methyl}-phenol (130106-85-3)

Guidance literature:

With sodium hydroxide; Multistep reaction; 1.) absolute methanol, room temp., 20 min., 2.) absolute ethanol, reflux;

Reference yield:

salicylaldehyde (90-02-8) + 4-methyl-5-<(2-aminoethyl)-thiomethyl>-imidazole (38585-67-0) → 2-{[(E)-2-(5-Methyl-3H-imidazol-4-ylmethylsulfanyl)-ethylimino]-methyl}-phenol (130106-85-3)

Guidance literature:

DOI:10.1039/DT9900002101

Reference yield: 80.0%

2-{[(E)-2-(5-Methyl-1H-imidazol-4-ylmethylsulfanyl)-ethylimino]-methyl}-phenol (130106-85-3) → 2-{[2-(5-Methyl-1H-imidazol-4-ylmethylsulfanyl)-ethylamino]-methyl}-phenol (147273-99-2)

Guidance literature:

With sodium tetrahydroborate; In ethanol; for 3h; Ambient temperature;

DOI:10.1039/DT9930000265

upstream raw materials:

salicylaldehyde

4-methyl-5-<(2-aminoethyl)-thiomethyl>-imidazole

2-[((5-methyl-1H-imidazol-4-yl)methyl)thio]ethanamine dihydrochloride

Downstream raw materials:

2-{[2-(5-Methyl-1H-imidazol-4-ylmethylsulfanyl)-ethylamino]-methyl}-phenol

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