1-(phthalimido)-4,8,12-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-15-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[2-(phenyl)benzyl]}amino-4,8,12-triazapentadecane

Base Information

Chemical Name:1-(phthalimido)-4,8,12-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-15-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[2-(phenyl)benzyl]}amino-4,8,12-triazapentadecane
CAS No.:868836-28-6
Molecular Formula:C₆₉H₈₃N₅O₁₀S₄
Molecular Weight:1270.71
Hs Code.:

1-(phthalimido)-4,8,12-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-15-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[2-(phenyl)benzyl]}amino-4,8,12-triazapentadecane

Synonyms:1-(phthalimido)-4,8,12-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-15-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[2-(phenyl)benzyl]}amino-4,8,12-triazapentadecane

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Chemical Property of 1-(phthalimido)-4,8,12-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-15-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[2-(phenyl)benzyl]}amino-4,8,12-triazapentadecane

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Technology Process of 1-(phthalimido)-4,8,12-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-15-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[2-(phenyl)benzyl]}amino-4,8,12-triazapentadecane

There total 4 articles about 1-(phthalimido)-4,8,12-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-15-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[2-(phenyl)benzyl]}amino-4,8,12-triazapentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 868836-27-5
1-(phthalimido)-4,8,12-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-15-N-[2,4,6-(trimethyl)benzenesulfonylamino]-4,8,12-triazapentadecane

: 868836-28-6
1-(phthalimido)-4,8,12-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-15-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[2-(phenyl)benzyl]}amino-4,8,12-triazapentadecane

Guidance literature:: 1-(phthalimido)-4,8,12-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-15-N-[2,4,6-(trimethyl)benzenesulfonylamino]-4,8,12-triazapentadecane; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃;

2-phenylbenzyl halide; In N,N-dimethyl-formamide;
DOI:10.1021/jm0505009

Reference yield: 65.0%

: 868836-28-6
1-(phthalimido)-4,8,12-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-15-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[2-(phenyl)benzyl]}amino-4,8,12-triazapentadecane

Guidance literature:

Reference yield:

: 5460-29-7
2-(3-bromopropyl)isoindole-1,3-dione

: 868836-28-6
1-(phthalimido)-4,8,12-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-15-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[2-(phenyl)benzyl]}amino-4,8,12-triazapentadecane

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / dimethylformamide / 0 °C

1.2: 65.7 percent / dimethylformamide

2.1: NaH / dimethylformamide / 0 °C

2.2: 65 percent / dimethylformamide

With sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1021/jm0505009