methyl 3-O-benzyl-2,4-dideoxy-2-C-methyl-4-C-methylene-6-O-trityl-α-D-arabino-hexopyranoside

Base Information

Chemical Name:methyl 3-O-benzyl-2,4-dideoxy-2-C-methyl-4-C-methylene-6-O-trityl-α-D-arabino-hexopyranoside
CAS No.:109914-96-7
Molecular Formula:C₃₅H₃₆O₄
Molecular Weight:520.668
Hs Code.:

Synonyms:methyl 3-O-benzyl-2,4-dideoxy-2-C-methyl-4-C-methylene-6-O-trityl-α-D-arabino-hexopyranoside

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Chemical Property of methyl 3-O-benzyl-2,4-dideoxy-2-C-methyl-4-C-methylene-6-O-trityl-α-D-arabino-hexopyranoside

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Technology Process of methyl 3-O-benzyl-2,4-dideoxy-2-C-methyl-4-C-methylene-6-O-trityl-α-D-arabino-hexopyranoside

There total 6 articles about methyl 3-O-benzyl-2,4-dideoxy-2-C-methyl-4-C-methylene-6-O-trityl-α-D-arabino-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2880-96-8,3150-15-0,3150-16-1,3257-59-8,14187-71-4,15384-57-3,19465-13-5,32976-15-1,52885-37-7,53270-02-3,53270-03-4,65391-11-9,65391-12-0,66537-92-6,67226-04-4,71184-14-0,86420-78-2,86420-79-3,91177-51-4,91177-52-5,117708-93-7,120408-72-2
methyl 2,3-anhydro-4,6-O-benzylidene-α-D-allopyranoside

: 109914-96-7
methyl 3-O-benzyl-2,4-dideoxy-2-C-methyl-4-C-methylene-6-O-trityl-α-D-arabino-hexopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 56 percent / Cu(I)I / diethyl ether / 5 h / 0 °C

2: 94 percent / NaH / tetrahydrofuran / 18 h / Heating

3: 85 percent / toluene-p-sulphonic acid monohydrate / methanol / 3 h / 0 °C

4: 95 percent / pyridine / 70 °C

5: oxalylchloride, DMSO / CH₂Cl₂ / 4 h / -60 °C

6: 84 percent / n-butyl-lithium / diethyl ether; hexane / 2 h / Heating

With copper(l) iodide; n-butyllithium; Chloro-oxo-acetic acid; sodium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; In tetrahydrofuran; pyridine; methanol; diethyl ether; hexane; dichloromethane;

Reference yield:

: 100-44-7
benzyl chloride

: 109914-96-7
methyl 3-O-benzyl-2,4-dideoxy-2-C-methyl-4-C-methylene-6-O-trityl-α-D-arabino-hexopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 94 percent / NaH / tetrahydrofuran / 18 h / Heating

2: 85 percent / toluene-p-sulphonic acid monohydrate / methanol / 3 h / 0 °C

3: 95 percent / pyridine / 70 °C

4: oxalylchloride, DMSO / CH₂Cl₂ / 4 h / -60 °C

5: 84 percent / n-butyl-lithium / diethyl ether; hexane / 2 h / Heating

With n-butyllithium; Chloro-oxo-acetic acid; sodium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; In tetrahydrofuran; pyridine; methanol; diethyl ether; hexane; dichloromethane;

Reference yield:

: 75837-44-4,109958-35-2,121467-57-0
methyl 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-C-methyl-α-D-altropyranoside

: 109914-96-7
methyl 3-O-benzyl-2,4-dideoxy-2-C-methyl-4-C-methylene-6-O-trityl-α-D-arabino-hexopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / toluene-p-sulphonic acid monohydrate / methanol / 3 h / 0 °C

2: 95 percent / pyridine / 70 °C

3: oxalylchloride, DMSO / CH₂Cl₂ / 4 h / -60 °C

4: 84 percent / n-butyl-lithium / diethyl ether; hexane / 2 h / Heating

With n-butyllithium; Chloro-oxo-acetic acid; toluene-4-sulfonic acid; dimethyl sulfoxide; In pyridine; methanol; diethyl ether; hexane; dichloromethane;